Water quality monitoring data sheet, May 2002

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Data File : C:\MSDCHEM\l\DATA\051302\11311.D Vial: 13 Acq On : 13 May 2002 9:36 pm Operator: Bohik / Inst 213 Sample : SAMPLE 11311 5/10/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\050802.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L

Peak Number 5 Heneicosane Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

18.30 0.10 ug/L 93776 Acenaphthene-dl0 18.21

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Heneicosane 296 C21H44 000629-94-7 83 2 Octadecane 254 C18H38 000593-45-3 78 3 Eicosane 282 C20H42 000112-95-8 78 4 Eicosane 282 C20H42 000112-95-8 78 Abundance Scan 796 (18.296 min): 11311.D (-) m/z 57.10 100.00% 57 85

5000 113 r 4) Per r 155 18.00 18.20 18.40 18.60

m/z-> 0 1’2’1111 l ............................................................ 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 m/z 71.10 97.99%

Abundance #245746: Heneicosane 43

5000 71 —4MAA 1 MyA 18.00 18.20 18.40 18.60 m/z 85.05 80.91% 99

m/z-> 0 mJ J J J 127 4 155 183 211 239 267 296 'l r rfi i " ■ ITT , if I rrt 11 b "Mrs I'l. n , I n I q ..!! |. I! 11.1 ■ 11. 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #193176: Octadecane 57 A . N... N..M,AA 18.00 18.20 18.40 18.60 5000 85 m/z 113.20 28.90% 4'1

113 ...

n/z-> O' MA4 11,141.169 197 225 254........ 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #228985: Eicosane 43 18.00 18'20 18'40 18.60 m/z 99.10 28.79% 71 5000

99 J . 127 155 183 211 239 282 0 fempp . fj ,|7... 111.11'> >>. ।. • • i • * m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 18.00 18.20 18.40 18.60

L1311.D 050802.M Tue May 14 11:10:35 2002 Page 7

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