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GCMS sample AE07115 results, April 25, 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis results for sample AE07115 including detection of unknown compounds.

NYC-WTC_000049063–000049101

Folder label: “GCMS X 4/12/02 A 4/23/02

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Scanned page image, NYC-WTC_000049081
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NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\l\DATA\041002\7115.D Vial: 22 Acq On : 11 Apr 2002 7:15 am Operator: Bohik Sample : SAMPLE 7115 3/27/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Heneicosane (CAS) $$ n-Hene... Concentration Rank 20

R.T. EstConc Area Relative to ISTD R.T.

22.63 2.69 ug/L 413127 Phenanthrene-dl0 22.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Heneicosane (CAS) $$ n-Heneicosane 296 C21H44 000629-94-7 74 2 Nonadecane 268 C19H40 000629-92-5 72 3 Pentadecane 212 C15H32 000629-62-9 68 4 Octacosane 394 C28H58 000630-02-4 68 Abundance Scan 3328 (22.633 min): 7115.D (-) m/ z 57.10 100.00%

AN 57 105

5000 85 MAP 4'1 183 22.40 22.60 22.80 23.00 246 m/z 105.10 90.48% 0 TTHT ‘ 1‘J‘‘‘l‘*/‘4**H********7****/** n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #245747: Heneicosane (CAS) $$ n-Heneicosane 57

5000 85 22.40 22.60 22.80 23.00 m/ z 71.10 58.06%

.AAa131,160,19729 wh IN 296 0+ m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #211482: Nonadecane 57 AM T T T T 22.40 22.60 22.80 23.00 5000 m/z: 43.10 42.69% 4'I 85

Tl/z-> 0 -- Abundance 1 113,141 169 197 WIPWmpg 225 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 #134012: Pentadecane 57 268 Aor AN 22.40 22.60 22.80 23.00 ' m/z: 85.15 40.90%

/z—> 5000

0J 4

M M444-Ant 85

113 141 169 212 . r.. 11... ।,. I.j.... ।. i.. 111111... । >. 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 HwN N 22.4022.60 22.80 23.00

7115.D 5080402BBC.M Tue Apr 23 15:52:48 2002 Page 4

NYC-WTC_000049081

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NYC-WTC_000049081Source: NYC Law Department, mirrored locally

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