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GCMS sample AE07110 results, April 25, 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis results for sample AE07110 including detection of unknown compounds.

NYC-WTC_000049027–000049062

Folder label: “GCMS X 4/12/02 A 4/23/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\041002\7110.D Vial: 17 Acq On : 11 Apr 2002 3:12 am Operator: Bohik Sample : SAMPLE 7110 3/27/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 4 Hexatriacontane Concentration Rank 16

R.T. EstConc Area Relative to ISTD R.T.

23.09 2.22 ug/L 286824 Phenanthrene-dl0 22.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 80 2 Pentatriacontane 493 C35H72 000630-07-9 80 3 Dotriacontane 451 C32H66 000544-85-4 80 4 Heneicosane (CAS) $$ n-Heneicosane 296 C21H44 000629-94-7 72 Abundance Scan 3406 (23.091 min): 7110.D (-) m/z 57.15 100.00%) 57

5000 85 4*1411*14444} Ti +}* > > : 1

miz-> 0- "LB 1, 1412149,18, ■ i • ‘ 1 ‘ i ■ ':•••• "* v J r | i i i I j I 22.80 23.00 23.20 23.40 m/z 71.10 52.35% t 50 100 150 200 250 300 350 400 450 Abundance #369892: Hexatriacontane 57

5000 85 "w22.80 23.00 23.20 23.40” m/z 43.10 44.43%

113,141 169 197 225 0- 1 30 1 1 ”l" +-*-** - tIIPII n/z-> 50 100 150 200 250 300 350 400 450 Abundance #367079: Pentatriacontane 517

22.80 23.00 23.20 23.40 5000 m/Z 55.10 37.25% 85

0- 100’13141,109,197 309 ..350........... 250 281300 150 200 225,253 400 450 miz-> 50 Abundance #355040: Dotriacontane 57 T T T T 22.80 23.00 23.20 23.40 m/z 85.20 34.41%

5000 85

Tl/z-> 1 113 , 1 1 il 141,169 197 225 253 281 309 337 365 393 421 450 0 —TTTn—TppfnfrftrTfTTTrejs 50i 100 150 200 250 300 350 400 450 MN22.80 23.00 23.20 23.40

7110.D 5080402BBC.M Tue Apr 23 15:52:11 2002 Page 6

NYC-WTC_000049045

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NYC-WTC_000049045Source: NYC Law Department, mirrored locally

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