GCMS surrogate recovery results, sample AE07115, April 15, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\041002\7115.D Vial: 22 Acq On : 11 Apr 2002 7:15 am Operator: Bohlk Sample ; SAMPLE 7115 3/27/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BB, M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 18 Hexatriacontane Concentration Rank 16

R.T. EstConc Area Relative to ISTD R.T.

36.68 . 14.90 ug/L 1376280 Perylene-dl2 34.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Heneicosane (CAS) $$ n-Heneicosane 296 C21H44 000629-94-7 91 3 Hexatriacontane $$ n-Hexatriacon. .. 507 C36H74 000630-06-8 90 4 Dotriacontane___________________________ 451 C32H66 000544-85-4 90 Abundance Scan 5719 (36.682 min); 7115.D (-) m/z 57.10 100.00% 57

5000 85

■n/z-> 0-

Abundance 0 w 50 1 100 ' ■ 150 200 I .... I.................................... ..............I, 250 ' 300 #369892: Hexatriacontane 350 ’ 400 450 m/z 36.40 36.60 36.80 37.00 71710 6^760%

57

5000 85 36.40 36.60 36.80 37.00 m/z 43.15 47761%

0- /zf ........... m/z-> 50 100 150 200 250 300 350 400 450 500 Abundance #245747: Heneicosane (CAS) $5 n-Heneicosane 57

36.40 36.60 36.80 37.00 5000 m/z 85.10 43.12% 85

Tl/Z-> Abundance 0- 0 w 50 239 100 150 200 250 300 350 400 450 296

#369895; Hexatriacontane $S n-Hexatriacontane 500 57 36.40 36.60 36.80 37.00 "in/z 55.10 2^739%

5000 85

29 0- ( ■n/z-> 0 50 100 150 200 250 300 350 400 450 500 36.40 36.60 36.80 37.00

'115.D 5080402BB.M Mon Apr 15 18:16:42 2002 Page 21

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