GCMS surrogate recovery results, sample AE07110, April 15, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

, Data File : C:\MSDCHEM\l\DATA\041002\7110.D Vial: 17 Acq On : 11 Apr 2002 3:12 am Operator: Bohlk Sample : SAMPLE 7110 3/27/02 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 Hexatriacontane Concentration Rank 16

R.T. EstConc Area Relative to ISTD R.T.

23.09 2.22 ug/L 286824 Phenanthrene-dl0 22.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 80 2 Pentatriacontane 493 C35H72 000630-07-9 80. 3 Dotriacontane 451 C32H66 000544-85-4 80 4 Heneicosane (CAS) $$ n-Heneicosane 296 C21H44 _____ 000629-94-7 72 Abundance Scan 3406 (23.091 min): 7110.D (-) m/z 57.15 100.00% 57

5000 85

113140 168 22.80 23.00 23.20 23.40 m/z 71.10 52.35% 0 fn/z-> 50 100 150 200 250 300 350 400 450 Abundance #369892: Hexatriacontane 57

5000 85 22.80 23.00 23.20 23.40 m/z 43.10 44.43%

0 30. 1 . ..................... m/z-> 50 100__ 150 200 250__ 300 350 400__ 450 Abundance #367079: Penta triacontane 57

22.80 23.00 23.20 23.40 5000 m/z 55.10 37.25%

0 1,1 -...................... m/z-> so' 100 150 200 250 ' 300 350 400 450 Abundance #355040: Dotriacontane 57 22.80 23.00 23.20 23.40 m/z 85.20 34.41%

5000 85

169.197 225 253 281 309 337 365 393 421 450 0 ' i'' ' I ' ' I ' ' ' ' I ' ' ' ' I ' m/z-> 50 100 150 200 250 300 350 400 450 22.80 23.00 23.20 23.40

7110.D 5080402BB.M Mon Apr 15 17:09:12 2002 Page 6

NYC-WTC_000061041