GCMS surrogate recovery results, sample AE07110, April 15, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\1\DATA\O41OO2\711O.D vial: 17 Acq On : 11 Apr 2002 3:12 am Operator: Bohlk Sample : SAMPLE 7110 3/27/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 1-Heptadecanol $$ n-Heptade... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

23.59 19.77 ug/L 2549600 Phenanthrene-dlO 22.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Heptadecanol $$ n-Heptadecanol. . . 256 C17H36O 001454-85-9 94 2 1-Hexadecanol 242 C16H34O 036653-82-4 94 3 Cyclododecane 168 C12H24 000294-62-2 94 4 Cyclotetradecane 196 C14H28 000295-17-0 93 Abundance Scan 3490 (23.585 min); 7110.D (-) m/z 55.10 100.00% 5(5 83 69 97 5000 4-

ill il 125 23.20 23.40 23.60 23.80 24,00 nil I A i 140153 168182196 m/z 57.10 90.03% 0 I yTi I T"| I r't I I 'Pl I' if I I ri I rl i r |"i 11 t । i i i i । i i ri j-r m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 ^bundance #195644: 1-Heptadecanol S$ n-Heptadecanol S$ Heptadecyl al... '56 4' 69 97 5000 T 111 23.20 23.40 23.60 23.80 24.00 m/z 83.10 79.59%

JdLU ^2® il', ■ A, I'l^-. ,, I I,, 0 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #177026; 1-Hexadecanol 43 , 57 83 23.20 23.40 23.60 23.80 24.00 70 97 m/z 69.10 71.88% 5000 29 111 125 Ji 139 154168182196 224 0 '■I *■' T ■ > ri I > I > > I. > < 11' I ■ 11111111 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #71567: Cyclododecane 41 5(5 23.20 2340 23.60 2^80 24 00 m/z 43.20 65.20% 69 83 97 111

4XW Uxx U-T 2? 168 14 I, 0 ''' I '' ■n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 23.20 23.40 23.60 23.80 24.00

7110.D 5080402BB.M Mon Apr 15 17:09:14 2002 Page 7

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