GCMS analysis report for sample AE07382, April 2002

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. Data File : C:\MSDCHEM\l\DATA\041802\7382.D Vial: 31 Acq On : 19 Apr 2002 10:16 am Operator: Bohlk Sample : SAMPLE 7382 3/28/02 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 Hexadecane (CAS) $$ n-Hexad... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

27.38 1.47 ug'/L 137536 Chrysene-dl2 30.14 .

Hit# of .5 Tentative ID MW MolForm CAS# Qual

1 Hexadecane (CAS) $$ n-Hexadecane... 226 C16H34 000544-76-3 78 2 Pentadecane (CAS) $$ n-Pentadecane 212 C15H32 000629-62-9 78 3 pentadecane _ 212 C15H32 000629-62-9 72 4 Heptadecane (CAS) $$ n-Heptadeca... 240 C17H36 000629-78-7 72 flibundance Scan 4136 (27.381 min): 7382.D (-) m/z 57.10 100.00% 5|7

43 71 5000 85

99 27.00 27.20 27.40 27.60 27.80

■n/z-> 0 I ' ' ' ' I 20 . 40 JuLj,JkXr 60 80 100 111 19K

120 140 160 iso 200 220 m/z 71.10 5^749%

Abundance #154903; Hexadecane (CAS) $$ n-Hexadecane $$ Cetane S$ n-C... 57

71

43 85 5000 2L00 27,20274027,6027^ m/z 43.20 53.60% 99

■n/z-> 0 I '''' I‘ 20 40 ■I ' ‘ 60 80 ' I ' ."1 /L/.r 100 120 140 160 180 200 . 5^.^. 220 Abundance #134014: Pentadecane (CAS) $5 n-Pentadecane 57 43

27.00 27.20 27.40 27.60 27.80 71 in/z 85.10 42723% 5000 '85

99 0 .l! . 212 'n/z-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #134045: pentadecane 57 43 27.00 27.20 27.40 27.60 27.80 m/z 55.10 22.58% 71 5000 85

0 'n/z-> 20 40 60 80 100 120 140 160 180 200 220 27.00 27.20 27.40 27.60 27.80'

7382.D 5080402BBC.M Tue Apr 23 19:05:20 2002 Page 7

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