GCMS surrogate recovery results, sample AE07110, April 15, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\l\DATA\041002\7110.D Vial: 17 Acq On : 11 Apr 2002 3:12 am Operator: Bohlk Sample : SAMPLE 7110 3/27/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080462BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 14 Octacosane (CAS) $$ n-Octac... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

31.45 19.95 ug/L 2393760 Chrysene-dl2 30.14

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Octacosane (CAS) $$ n-Octacosane 394 C28H58 000630-02-4 91 2 Heptacosane 380 C27H56 000593-49-7 91 3 Octacosane 394 C28H58 000630-02-4 90 4 Tetracosane (CAS) $$ n-Tetracosane 338 C24H50 _____ 000646-31-1 90 <\bundance Scan 4829 (31.452 min): 7110.D (-) m/z 57.10 100.00% 57

5000 85

J<- ' I ' ' ' ' I 31.20 31.40 31.60 31.80 253 ................................... m/z 71.10 61.19% 0 m/z-> 50 100 150 200 250 300 350 400 Abundance #329269: Octacosane (CAS) $S n-Octacosane 5(7

85 7 5000 31.20 31.40 31.60 31.80 m/z 43.10 42.96%

0^ J rXj ■ J J H L yf ■n/z-> 50 100 150 200 250 300 350 400 Abundance #320678: Heptacosane 57 7 31.20 31.40 31.60 31.80 TililB m/z 85.10 42.37% 85

0 ' ' I ' I 197 225 253 281 309 337 380 m/z-> 50 100 150 200 250 300 350 400 Abundance #329267: Octacosane 7 31.20 31.40 31.60 31.80 m/z 55.10 21.54%

5000 85

29

n/z-> 0 Ai 50 i, 100 w' 200 253 281 309 337 365 394 250 300 350 400 31.20 31.40 31.60 31.80

7110.D 5080402BB.M Mon Apr 15 17:09:24 2002 Page 16

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