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GCMS sample AE07110 results, April 25, 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis results for sample AE07110 including detection of unknown compounds.

NYC-WTC_000049027–000049062

Folder label: “GCMS X 4/12/02 A 4/23/02

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Scanned page image, NYC-WTC_000049055
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\041002\7110.D Vial: 17 Acq On : 11 Apr 2002 3:12 am Operator: Bohik Sample : SAMPLE 7110 3/27/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 14 Octacosane (CAS) $$ n-Octac... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

31.45 19.95 ug/L 2393760 Chrysene-d12 30.14

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Octacosane (CAS) $$ n-Octacosane 394 C28H58 000630-02-4 91 2 Heptacosane 380 C27H56 000593-49-7 91 3 Octacosane 394 C28H58 000630-02-4 90 4 Tetracosane (CAS) $$ n-Tetracosane 338 C24H50 000646-31-1 90 Abundance Scan 4829 (31.452 mln): 7110.D (-) m/z 57.10 100.00% 57

5000 85 ------ ) “— .... ~ 31.20 31.40 31.60 31.80 0- Pr ,11,413147,, ,198211 253.............. m/z 71.10 61.19% miz-> 50 100 150 200 250 300 350 400 Abundance #329269: Octacosane (CAS) $$ n-Octacosane 57

5000 85 T T T T 31.20 31.40 31.60 31.80 m/z 43.10 42.96%

0- J • 1 i J 1,1112141,169/197,225,253,281309, , 394 miz-> 50 100 150 200 250 300 350 400 Abundance #320678: Heptacosane 57 J T T T T 31.20 31.40 31.60 31.80 5000 m/z 85.10 42.37% 85

29 0- .1 A " 1,1113,141 169 197 225 253 281 309 337 380 miz-> 50 100 150 200 250 300 350 400 Abundance #329267: Octacosane 57 T T T TTT 31.2031.40 31.60 31.80 m/z 55.10 21.54%

5000 85

29 0 /:11334141.169,197,225,253 281 309 337 365 394 T ‘I T •n/z-> 50 100 150 200 250 ' 300 350 400 31.20 31.40 31.60 31.80

7110.D 5080402BBC.M Tue Apr 23 15:52:23 2002 Page 16

NYC-WTC_000049055

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NYC-WTC_000049055Source: NYC Law Department, mirrored locally

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