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GCMS sample AE07110 results, April 25, 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis results for sample AE07110 including detection of unknown compounds.

NYC-WTC_000049027–000049062

Folder label: “GCMS X 4/12/02 A 4/23/02

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Scanned page image, NYC-WTC_000049056
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data Pile : C:\MSDCHEM\l\DATA\041002\7110.D Vial: 17 Acq On : 11 Apr 2002 3:12 am Operator: Bohik Sample : SAMPLE 7110 3/27/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 15 Heptacosane Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

32.37 21.77 ug/L 1992310 Perylene-dl2 34.01

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptacosane 380 C27H56 000593-49-7 91 2 Octacosane $$ n-Octacosane 394 C28H58 000630-02-4 91 3 Heneicosane $$ n-Heneicosane 296 C21H44 000629-94-7 90 4 Pentacosane $$ n-Pentacosane 352 C25H52 000629-99-2 90 Abundance Scan 4986 (32.375 min): 7110.D (-) m/z 57.10 100.00% 57

5000 85

32.00 32.20 32.40 32.60 0- — —1 j 11134141,169,197 225 267 295 m/z 71.10 59.98% • 1 । 1 1 1 ■ r miz-> 50 100 150 200 250 300 350 400 Abundance #320678: Heptacosane F7

5000 85 32.00 32.20 32.40 32.60 m/z 43.15 44.43% 29 | J,J1J3J141 169 197 225 253 281 309 337 380 0- I . ‘ ■ " r i fn/z-> 50 100 150 200 250 300 350 400 Abundance #329266: Octacosane $$ n-Octacosane 57

T T T T 1‘ 32.00 32.20 32.40 32.60 m/z 85.10 42.46% 5000 85

29 113 1 J 141,169 197 225 253 281 309 337 365 394 0- ’ t ■ ' -2*tm m/z-> 50 100 150 200 250 300 350 400 Abundance #245745: Heneicosane $$ n-Heneicosane wPW 57 32.00 32.20 32.40 32.60 T m/z 55.10 23.21%

85 5000

29 . ........................................................................................ AWvw 0 •" * " ‘I T T T 18 Ti/z-> 50 100 150 200 250 300 350 400 32.00 32.20 32.40 32.60

7110.D 5080402BBC.M Tue Apr 23 15:52:24 2002 Page 17

NYC-WTC_000049056

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NYC-WTC_000049056Source: NYC Law Department, mirrored locally

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