GCMS sample AE07115 results, April 25, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\1\DATA\041002\7115.D Vial: 22 Acq On : 11 Apr 2002 7:15 am Operator: Bohik Sample : SAMPLE 7115 3/27/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 15 Heptacosane Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

34.13 47.78 ug/L 4413600 Perylene-dl2 34.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Heptacosane 380 C27H56 000593-49-7 91 2 Tetracosane (CAS) $$ n-Tetracosane 338 C24H50 000646-31-1 91 3 Heneicosane $$ n-Heneicosane 296 C21H44 000629-94-7 91 4 Hexatriacontane $$ n-Hexatriacon... 507 C36H74 000630-06-8 90 Abundance Scan 5285 (34.132 min): 7115.D (-) m/z 57.10 100.00% 57

5000 85

33.80 34.66 34.20 34.40 ' ~ — J1 113 l j| 141.169 197 225 253 281 309 m/z 71.10 61.65% 0- m/z-> 50 100 150 200 250 300 350 Abundance #320678: Heptacosane 57

-—R 5000 85 33‘66 34'66 34.20 34.40 m/z 85.10 43.54% 29 0- 4 14J ^,1^9.197 225 253 281 309 337 , 380, Tl/Z-> 50 100 150 200 250 300 350 Abundance #288787: Tetracosane (CAS) $5 n-Tetracosane 57

33.80 34.00 34.20 34.40 5000 85 m/z 43.20 41.92%

1113 0- • ■ i ■ II 1,1141.169,197,225 253 281 309 338 , , m/z-> 50 100 150 ' ' 200 ' 250 300 350 Abundance #245745: Heneicosane $$ n-Heneicosane 57 •11 ■'' ■ i ■' ■ ‘ i ■ ■' ■ i • • ■ ■ i 33.80 34.00 34.20 34.40 m/z 55.10 23.38%

85 5000

29 I113 . 1 J ,7,169 197 225 253 296 0 —4—f-r-r 1 Pi" 1 1*1 1 !»■ [ ‘| t r. i rn-1 ■ *| I I I r I I I •n/z-> 50 100 150 200 250 300 350 33.80 34.66 34'20 34.40 1

7115.D 5080402BBC.M . Tue Apr 23 15:53:05 2002 Page 18

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