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GCMS sample AE07110 results, April 25, 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis results for sample AE07110 including detection of unknown compounds.

NYC-WTC_000049027–000049062

Folder label: “GCMS X 4/12/02 A 4/23/02

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Scanned page image, NYC-WTC_000049057
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\041002\7110.D vial: 17 Acq On : 11 Apr 2002 3:12 am Operator: Bohik Sample : SAMPLE 7110 3/27/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 16 Tetracosane (CAS) $$ n-Tetr... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

33.27 16.71 ug/L 1529330 Perylene-d12 34.01 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetracosane (CAS) $$ n-Tetracosane 338 C24H50 000646-31-1 91 2 Octacosane 394 C28H58 000630-02-4 91 3 Heptacosane 380 C27H56 000593-49-7 91 4 Octacosane (CAS) $$ n-Octacosane 394 C28H58 000630-02-4 91 Abundance Scan 5138 (33.268 min): 7110.D (-) m/z 57.10 100.00% 57

5000 85 P T TT T T 33.00 33.20 33.40 33.60

rn/z-> 0- — 11,11244119,19622% m/z 71.10 62.05% 50 100 . 150 200 250 300 350 Abundance #288787: Tetracosane (CAS) $$ n-Tetracosane 57

5000 85 ‘ 33.00 33.20 33.40 33.607 m/z 85.10 44.94% 113 0- |IIi TdrT ——1141,169 197 225 253 281 309 338 HRdkmuTTTTTTUTT ‘ 'I m/z-> 50 100 150 200 250 300 350 Abundance #329267: Octacosane 57 33.00 33.20 33.40 33.60 5000 m/z 43.10 44.22% 85

29 J 1113,141 169 197 225 253 281 309 337 365 394 0- TI8 1ddd2—n18mB/0d—da8n—-m0n———n——]- m/z-> 50 100 150 200 250 300 350 Abundance #320678: Heptacosane 57 ' 33*00 33.20 33.4033.60” m/z 55. 10 20.44%

5000 85

291 1 1,41134141,169.197.225,253281309337,380 0 44 11*. T T /z—> 50 100 150 200 250 300 350 1 33.00 33.20 33.40 33.60

7110.D 5080402BBC.M Tue Apr 23 15:52:25 2002 Page 18

NYC-WTC_000049057

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NYC-WTC_000049057Source: NYC Law Department, mirrored locally

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