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GCMS sample AE07110 results, April 25, 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis results for sample AE07110 including detection of unknown compounds.

NYC-WTC_000049027–000049062

Folder label: “GCMS X 4/12/02 A 4/23/02

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Scanned page image, NYC-WTC_000049058
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NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\1\DATA\041002\7110.D Vial: 17 Acq On : 11 Apr 2002 3:12 am Operator: Bohik Sample : SAMPLE 7110 3/27/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 17 Tetracosane (CAS) $$ n-Tetr... Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

34.13 11.95 ug/L 1094270 Perylene-d12 34.01

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetracosane (CAS) $$ n-Tetracosane 338 C24H50 000646-31-1 91 2 Heneicosane $$ n-Heneicosane 296 C21H44 000629-94-7 91 3 Octacosane (CAS) $$ n-Octacosane 394 C28H58 000630-02-4 91 4 Octacosane 394 C28H58 000630-02-4 90 Abundance Scan 5285 (34.132 mln): 7110.D (-) m/z 57.10 100.00% 57

5000 85

• ■ i ■ ■ • ■ i ‘ ■ i • • • •) ‘■ i 33.80 34.00 34.20 34.40

m/z~> 0- “50I18,1134147.189/ 100 150 211........................................... m/z 71.10 61.87% 200 250 300 350 400 Abundance #288787: Tetracosane (CAS) $$ n-Tetracosane 57

85 J PArr 5000 33.80 34.00 34.20 34.40 11 m/z 85.10 41.69% 1 113 I | I J 141,169 197 225 253 281 309 338 0- • • i 4 f . ■ । r ■ . r । * » fay r • • » ( । । i • । * i 1* । ri । r । ■ m/z-> 50 100 150 200 250 300 350 400 Abundance #245745: Heneicosane $$ n-Heneicosane 57

1 ■ i ■ T T T T 85 33.80 34.00 34.20 34.40 5000 m/z 43.10 38.62%

29 113 1 * * 1 Ikj 1141,169 197 225 253 296 0- . r. r . , 1 | rl ’ I : 1 । rj m/z-> 50 100 150 200 250 300 350 ' 400 Abundance #329269: Octacosane (CAS) $$ n-Octacosane 57 T T T T T 33.80 34.00 34.20 34.40 m/z 55.10 20.91%

5000 85

walywd P ■ ' |* 1,11133417,169,197/225,253,281.309, . 394 T T T T T m/z—> 50 100 150 200 250 300 350 400 33.80 34.00 34.20 34.40

7110.D 5080402BBC.M Tue Apr 23 15:52:27 2002 Page 19

NYC-WTC_000049058

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NYC-WTC_000049058Source: NYC Law Department, mirrored locally

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