GCMS sample AE07110 results, April 25, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\041002\7110.D Vial: 17 Acg On : 11 Apr 2002 3:12 am Operator: Bohik Sample : SAMPLE 7110 3/27/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 18 Pentatriacontane Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 34.97 7.41 ug/L 677842 Perylene-dl2 34.01 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Pentatriacontane 493 C35H72 000630-07-9 91 2 Hexatriacontane 507 C36H74 000630-06-8 91 3 Tetratriacontane $$ n-Tetratriac... 479 C34H70 014167-59-0 90 4 Tetratetracontane 619 C44H90 007098-22-8 90 Abundance Scan 5427 (34.966 min): 7110.D (-) m/z 57.10 100.00% 57

5000 85

34*60 34.80 35.00 35.20 ~

/z—> 0- 0 — 50 100 413141150....................... 200 250 300 350 400 , m/z 71.10 58.91%

Abundance #367079: Pentatriacontane 57

MAmud 5000 85 Ti T T T iT 34.60 34.80 35.00 35.20 m/z 85.15 42.83% 1 113 0- .1)" .+8,14.141169197,225,253 281 309 . m/z-> 0 50। 100 150 200 250 300 350 400 Abundance #369892: Hexatriacontane 57 MW/tw "Mna-t 34.60 34.80 35.00 35.20 5000 m/z 43.10 39.80% 85

+30 d" 113 141 169 197 225 0- Pif .1 f |'» 1 far rfi > । > । i । । i । i i । । i i । । । » n/z-> 0 50 100 150 200 250 300 350 400 Abundance #363627: Tetratriacontane $$ n-Tetratriacontane 57 34*60 34.80 35.00 35.20 ' T m/z 55.10 22.84%

5000 85

29 113

miz—> 0- 0 LT 44 ' j 141 169 197 225 253 281 311337 367 410435 50 100 64" Pi 1 Pit *4* (ti * ii 1 p 150 200 250 300 350 1 I I i l l . 400 ‘I T T T 34.60 34.80 35.00 35.20 I’

7110.D 5080402BBC.M Tue Apr 23 15:52:28 2002 Page 20

NYC-WTC_000049059