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GCMS sample AE07115 results, April 25, 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis results for sample AE07115 including detection of unknown compounds.

NYC-WTC_000049063–000049101

Folder label: “GCMS X 4/12/02 A 4/23/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\041002\7115.D Vial: 22 Acq On : 11 Apr 2002 7:15 am Operator: Bohik Sample : SAMPLE 7115 3/27/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 17 Hexatriacontane Concentration Rank 14

R.T. EstConc Area Relative to ISTD R.T.

35.78 22.39 ug/L 2068010 Perylene-dl2 34.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Octacosane 394 C28H58 000630-02-4 91 3 Heptacosane 380 C27H56 000593-49-7 91 4 Tetracosane (CAS) $$ n-Tetracosane 338 C24H50 000646-31-1 90 Abundance Scan 5566 (35.783 min): 7115.D (-) m/z 57.10 100.00%) 57

5000 85

35.40 35.60 35.80 36.00 36.20 0- TId" 1134141199, 197,225,258, ■ ■ i ■ ‘ ■ i ■ ■ ■ ■ i m/z 71.10 57.34% tn/z-> 50 100 150 200 250 300 350 Abundance #369892: Hexatriacontane 57

5000 T T T T 85 35.40 35.60 35.80 36.00 36.20 m/z 43.10 42.13%

1 1113,141 169 197 225 0- 30, r TTT Pi" f 11m । i ■! 1 1 [ 1 ■ 1 1 । ■ 1 i f n/z-> 50 100 150 200 250 300 350 Abundance #329267: Octacosane 57

35.40 35*60 35.80 36.00 36.20 5000 m/z 85.10 40.01% 85

29 I , 113 0- ■ I ■ 44,4.4, 141 169 197 225 253 281 309 337 365 394 . f ! . I r .‘l r . • I 1 I I b 7 . I > r I I I I -I IIT

miz-> 50 100 150 200 250 300 350 -MMWo Abundance #320678: Heptacosane 57 35'46 35.60 35.80 36.00 36.20 m/z 55.10 21.96%

5000 85

29 0 ,1‘ r i ' 1,4113141 169/197,225,253 281 309 337.380 , i m/z-> 50 100 150 200 250 '360 3501 i i i 35.40 35.60 35.80 36.00 36.20

7115.D 5080402BBC.M Tue Apr 23 15:53:07 2002 Page 20

NYC-WTC_000049097

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NYC-WTC_000049097Source: NYC Law Department, mirrored locally

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