GCMS sample AE07115 results, April 25, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\041002\7115.D Vial: 22 Acq On : 11 Apr 2002 7:15 am Operator: Bohik Sample : SAMPLE 7115 3/27/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L Peak Number 16 Hexatriacontane Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

34.97 35.89 ug/L 3315840 Perylene-d12 34.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Octacosane 394 C28H58 000630-02-4 91 3 Tetracosane (CAS) $$ n-Tetracosane 338 C24H50 000646-31-1 91 4 Heptacosane 380 C27H56 000593-49-7 91 Abundance Scan 5427 (34.966 min): 7115.D (-) m/z 57.10 100.00% 57

5000 85

34.60 34.80 35.00 35.20 P .0- — I +.41113 #,+141.169197 225.253 281 • * । * * * * । m/z 71.10 63.09% m/z-> 50 100 150 200 250 300 350 Abundance #369892: Hexatriacontane £7

5000 ’T’1661111177rrTrt’1R 85 34.60 34.80 35.00 35.20 m/z 85.10 43.88%

0* 30, 1 ” i 1 1,41134141,189,197,225, .J m/z-> 50 100 150 200 250 300 350 Abundance #329267: Octacosane 57

34.60 34.80 35.00 35.20 5000 m/z 43.15 42.04% 85

29 J 1113,141169 197 225 253 281 309 337 365 394 —4 TIY 0- —"* CT C > "i rr-| >ii-i । ri । Tl/Z-> 50 100 150 200 250 300 350 Abundance #288787: Tetracosane (CAS) $$ n-Tetracosane 57 TT T T T T8 34.60 34.80 35.00 35.20 m/z 55.10 22.65%

5000 85

i 1113 0 I I II il 141,169 197 225 253 281 309 338 • 'I 1 " 1 > 1 1 ’ i 1 ■ 1 '"i f ‘-i -i I*I r ITr । ri । i । । i । m/z—> 50 100 150 200 250 300 350 34.60 34.80 35.00 35.20 R

7115.D 5080402BBC.M Tue Apr 23 15:53:06 2002 Page 19

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