GCMS surrogate recovery results, sample AE07115, April 15, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\041002\7115.D Vial: 22 Acq On : 11 Apr 2002 7:15 am Operator: Bohlk Sample : SAMPLE 7115 3/27/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 17 Hexatriacontane Concentration Rank 14

R.T. EstConc Area Relative to ISTD R.T.

35.78 22.39 ug/L 2068010 Perylene-dl2 34.02

Hit# Of 5 Tentative ID MW MolForm CAS# . Qual

1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Octacosane ' 394 C28H58 000630-02-4 91 3 Heptacosane 380 C27H56 000593-49-7 91 4 Tetracosane (CAS) $$ n-Tetracosane 338 C24H50 000646-31-1 90 Abundance Scan 5566 (35.783 min): 7115.D (-) m/z 57.10 100.00% 57

5000 85

35 40 35.60 35.80 36.00 36.20 0 m/z 71710 57734% ■n/z-> 50 100 150 200 250 300 350 Abundance #369892: Hexatriacontane ^•7

5000 85 35.40 35.60 35.80 36.00 36.20 m/z 43.10 42.13%

30 0 ■n/z-> 50 100 150 200 250 300 350 Abundance #329267: Octacosane 57

35.40 35.60 35.80 36.00 36.20 5000 m/z85.10 40.01% 85

29 I 0 ■n/z-> 50 100 150 200 250 ' ' 300 ' ' 'sM ~ Abundance #320678: Heptacosane 57 35 40 35.60 35.80 36.00 36.20 m/z 55710 21.96%

SB 85

0 .TIjj ■< ?y, ■n/z-> 50 100 150 200 250 300 350 35.40 35.60 35.80 36.00 36.20

7115.D 5080402BB.M Mon Apr 15 18:16:41 2002 Page 20

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