GCMS surrogate recovery results, sample AE07110, April 15, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\l\DATA\041002\7110.D Vial: 17 Acq On : 11 Apr 2002 3:12 am Operator: Bohlk Sample : SAMPLE 7110 3/27/02 Inst : Instrumen Mise : I Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 18 Pentatriacontane Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T. I 34.97 7.41'ug/L 677842 Perylene-dl2 34.01

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pentatriacontane 493 C35H72 000630-07-9 91 2 Hexatriacontane 507 C36H74 000630-06-8 91 3 Tetratriacohtane $$ n-Tetratriac... 479 C34H70 014167-59-0 .90 4 Tetratetracontane 619 C44H90 007098-22-8 90 Abundance Scan 5427 (34.966 min): 7110.D (-) m/z 57.10 100.00% 57

lililil 85

34.60 34.80 35.00 35.20 207 m/z 71.10 58.91% 0- m/z-> 0 50I ,100 150 200 250 300 350 400 Abundance #367079; Pentatriacontane 5?

5000 85 34.60 34.80 35.00 35.20 m/z 85.15 42.83% 113 0- 255^3 281 309 , ......... nn/z-> 0 50 ,100 150 200 250 300 350 400 Abundance #369892: Hexalriacontane 57 ... 34.60 34.80 35.00 35.20 5000 m/z 43.10 39.80% 85

. 0- m/z-> 0 50 100 150 200 250 300 350 400 Abundance #363627: Tetratriacontane $$ n-Tetratriacontane —T-p-rr-r-p-TT- 5(7 34.60 34.80 35.00 35.20 m/ z 55.10 22.84%

5000 85

nn/z-> 0 - 0 29

50 I too 150 200 250 300 350 400 34.60 34.80 35.00 35.20

7110.D 5080402BB.M Mon Apr 15 17:09:29 2002 Page 20 I ___________________ L NYC-WTC_000061055