GCMS sample AE07110 results, April 25, 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\041002\7110.D Vial: 17 Acq On : 11 Apr 2002 3:12 am Operator: Bohlk Sample : SAMPLE 7110 3/27/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 20 Tetratriacontane $$ n-Tetra... Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T.

36.68 2.27 ug/L 208179 Perylene-dl2 34.01

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetratriacontane $$ n-Tetratriac... 479 C34H70 014167-59-0 80 2 Octacosane $$ n-Octacosane 394 C28H58 000630-02-4 80 3 Octacosane 394 C28H58 000630-02-4 74 4 Heneicosane (CAS) $$ n-Heneicosane 296 C21H44 000629-94-7 74 Abundance Scan 5719 (36.682 mln): 7110.D (-) m/z 57.10 100.00% 57

5000 85 Myo 113 141 36.40 36.60 36.80 37.00

miz-> 0 0 —4 50 100 150 200 208 ■ i ■ 1 • • i ■ ■ ■ ■ i ■ ■ • • i ■ ■ 250 300 350 400 ■ i • • m/z 71.15 60.44%

Abundance #363627: Tetratriacontane $$ n-Tetratriacontane 57

MWWkw 5000 85 36.40 36.60 36.80 37.00 m/z 85.15 36.27% 29 1 i 113

m/z-> 0- 0 4100 4A 1,141169197 225 253 281 311 337 367,410435 50 150 200 250 300 350 400 Abundance #329266: Octacosane $$ n-Octacosane 57 ‘Whew 36.40 36.60 36'80 37.00 TT 5000' 85 m/z 43.20 32.96%

29 । 113 "Li I) | 111,169,197 225 253 281 309 337 365 394 Tl/z-> Abundance 0- 0 50 ' 100 150 200 250 300 350’ 400 #329268: Octacosane MM 57 T T T 36.40 36.60 36.80 37.00 m/z 55.10 31.76%

5000 85

113

0- — L J 1.141 .183 211 239 267 309 337 , . 394 ■ ■ i ■ ■ •' i • ■ ■ ‘ i' • • ■ i • ■ m/z—> 0 50 100 150 200 250 300 350 400 36.40 36.60 36.80 37.00

7110.D 5080402BBC.M Tue Apr 23 15:52:30 2002 Page 22

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