GCMS surrogate recovery results, sample AE07115, April 15, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\041002\7115.D Vial: 22 Acg On : 11 Apr 2002 7:15 am Operator: Bohllc Sample : SAMPLE 7115 3/27/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

■ Peale Number 16' Hexatriacontane Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

34.97 35.89 ug/L 3315840 Perylene-dl2 34.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Octacosane 394 C28H58 .000630-02-4 91 3 Tetracosane (CAS) $$ n-Tetracosane 338 C24H50 000646-31-1 91 4 Heptacosane 380 C27H56 000593-49-7 91 Abundance Scan 5427 (34.966 min): 7115.D (-) m/z 57.10 100.00% 57

5000 85

I I 1113 3£603<8035,0035.20 , H 1| j141 169 197 225 253 281________ m/z 71.10 63.09% 0^ ■1 T r, q r . , r , , i r-1 • । i pi । । । । । । । । । । m/z-> 50 100 150 200 250 300 350 Abundance #369892: Hexatriacontane 57

5000 85 34.60 34.80 35.00 35.20 m/z 85.10 43.88%

30 11 197 225 0^ T , , I r, , f i'. , I f I■ I I I I I I I I I I I , I I m/z-> 50_ 100 150 200 250 300 350 Abundance #329267: Octacosane 5*7

34.60 34.80 35.00 35.20 liwa m/z 43.15 42.04% 85

m/z-> 0^ ijj 50 i 100 150 200 225 253 281 309 337 365 394 250 300 350 . Abundance #288787: Tetracosane (CAS) $S n-Tetracosane 57 34.60 34.80 35.00 35.20 m/z 55.10 22.65%

'n/z-> SEE

0 50 85

jJT ,141 169 197^^5 253 281 309 338 100 150 200 250 300 350 JU 34.60 34.80 35.00 35.20

7115.D 5080402BB.M Mon Apr 15 18:16:40 2002 Page 19

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