GCMS surrogate recovery results, sample AE07115, April 15, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\041002\7115.D vial: 22 Acq On : 11 Apr 2002 7:15 am Operator: Bohllc Sample : SAMPLE 7115 3/27/02 Inst ; Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 15 Heptacosane Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

34.13 47.78 ug/L 4413600 Perylene-dl2 34.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual.

1 Heptacosane 380 C27H56 000593-49-7 91 2 Tetracosane (CAS) $$ n-Tetracosane 338 C24H50 000646-31-1 91 3 Heneicosane $$ n-Heneicosane 296 C21H44 000629-94-7 91 4 Hexatriacontane $$ n-Hexatriacon... 507 C36H74 000630-06-8 90 Abundance Scan 5285 (34.132 min): 7115.D (-) m/z 57.10 100.00% 57

' 5000 85

33.80 34.00 34.20 34.40 0 1 J 253 ,281 309 . m/z 71.10 61.65% ■n/z-> 50 100 150 200 250 300 350 Abundance #320678; Heptacosane 5l7

5000 85 33.80 34.00 34.20 34.40 m/z 85.10 43.54% 29 11 169.197 ^5 253 281 309 337 380 0 X 50 160 ' 150 ' ' '260 '250 ' ' '360 ' '350 ' ■n/z-> Abundance #288787: Tetracosane (CAS) SS n-Tetracosane 5/

33.80 34.00 34.20 34.40 5000 85 m/z 43.20 41.92%

0 'n/z-> 50 100 150 200 250 300 350 Abundance #245745: Heneicosane $$ n-Heneicosane 57 33.80 34.00 34.20 34.40 m/z 55.10 23.38% 85 ssa 29 1 0 Xlr J 197^^5 253 296 33.80 ^.00 34'20 ^.46 n/z-> 50 100 150 200 250 300 350

7115.D 5080402BB.M Mon Apr 15 18:16:39 2002 Page 18

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