GCMS surrogate recovery results, sample AE07110, April 15, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\l\DATA\041002\7110.D Vial: 17 Acq On : 11 Apr 2002 3:12 am Operator: Bohllc Sample : SAMPLE 7110 3/27/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peale Number 13 Heptacosane Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

30.49 20.63 ug/L 2476070 Chrysene-dl2 30.14

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptacosane 380 C27H56 000593-49-7 91 2 Eicosane 282 C20H42 000112-95-8 91 3 Tetracosane (CAS) $$ n-Tetracosane 338 C24H50 000646-31-1 90 4 Octacosane (CAS) $$ n-Octacosane 394 C28H58 _____ 000630-02-4 90 Abundance Scan 4665 (30.489 min): 7110.D (-) m/z 57.10 100.00% 7

5000 85

j JiJj 169/197 239 281 352 30.20 30.40 30.60 30.80 0^ m/z 71.10 58.25% m/z-> I^___Z1OO__15O__3 oO___25o2ZZ3^^ Abundance #320678: Heptacosane 57

5000 85 30.20 30.40 30.60 30.80 m/z 43.20 41.71%

m/z-> Abundance 29 01 .! 50 100 150 200 #228992: Eicosane 250 300 350___ I 30.20 30.40 30.60 30.80 5000 m/z 85.15 41.15% 85 29

a A ,1, ................... 282 0 ■n/z-> 50 100 150 200 250 300 350 Abundance #288787; Tetracosane (CAS) $S n-Tetracosane 30.20 30.40 30.60 30.80 m/z 55.10 20.61%

5000 85

113 il j/'l''J69.197 225 253 281 309 338 0 ' ' ' M ' 'l ' I ' ' ' ' I ' ' ' ' I [n/z-> 50 100 150 200 250 300 350 30.20 30.40 30.60 30.80

7110.D 5080402BB.M Mon Apr 15 17:09:23 2002 Page 15

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