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GCMS sample AE07110 results, April 25, 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis results for sample AE07110 including detection of unknown compounds.

NYC-WTC_000049027–000049062

Folder label: “GCMS X 4/12/02 A 4/23/02

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Scanned page image, NYC-WTC_000049051
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\041002\7110.D Vial: 17 Acq On : 11 Apr 2002 3:12 am Operator: Bohlk Sample : SAMPLE 7110 3/27/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 10 Heptacosane Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

27.37 12.57 ug/L 1508300 Chrysene-dl2 30.14

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptacosane 380 C27H56 000593-49-7 91 2 Tricosane (CAS) $$ n-Tricosane 324 C23H48 000638-67-5 91 3 Eicosane 282 C20H42 000112-95-8 91 4 Pentadecane 212 C15H32 000629-62-9 87 Abundance Scan 4135 (27.375 min): 7110.D (-) m/z 57.10 100.00% 57

5000 85 >—y TT i ■ • • • । T It — 113 27.00 27.20 27.40 27.60 0- 1 j j4 4141.169197 225 253 .... . m/z 71.10 60.13% m/z-> 50 100 150 200 250 300 350 Abundance #320678: Heptacosane 57

— 5000 Ti T 1***1 Tr 85 27.00 27.20 27.40 27.60 m/z 43.15 44.84% 29 0- 1i 4,41134141.169, 197,225,253 281 309 337 . 380 n/z-> 50 100 ' ‘ ‘l50 ' ‘260' ‘ ‘ 250 ' ' ‘360' ‘ ‘ 350' Abundance #275685: Tricosane (CAS) $$ n-Tricosane 57

27.00 27.20 27.40 27'60 5000 85 m/z 85.10 42.53%

113 28, .1 J , 1. 141:169, . ,211.239 267 295 324 0- ,44-T ■ i ‘ 1 m/z-> 50 100 150 200 250 300 350 Abundance #228992: Eicosane 57 27.00 27*20 2740 27.60 ~ m/z 55.10 20.00%

5000 85 29

0 1 , ’ ’ 1 1 A 1113,141 169..... 282 m/z—> 50 100 150 200 250 300 ‘ ' 350 27.00 27.20 27.40 27.60 T

7110iD 5080402BBC.M Tue Apr 23 15:52:18 2002 Page 12

NYC-WTC_000049051

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NYC-WTC_000049051Source: NYC Law Department, mirrored locally

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