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GCMS sample AE07110 results, April 25, 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis results for sample AE07110 including detection of unknown compounds.

NYC-WTC_000049027–000049062

Folder label: “GCMS X 4/12/02 A 4/23/02

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NYC 9/11 Public Portal Document Library Search Compound Report

. Data File : C:\MSDCHEM\1\DATA\041002\7110.D Vial: 17 Acq On : 11 Apr 2002 3:12 am Operator: Bohik Sample : SAMPLE 7110 3/27/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 11 Eicosane Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

28.46 17.77 ug/L 2132650 Chrysene-dl2 30.14

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Eicosane 282 C20H42 000112-95-8 91 2 Hexadecane 226 C16H34 000544-76-3 90 3 Heneicosane $$ n-Heneicosane 296 C21H44 000629-94-7 90 4 Heptadecane (CAS) $$ n-Heptadeca... 240 C17H36 000629-78-7 90 Abundance Scan 4319 (28.456 min): 7110.D (-) m/z 57.10 100.00% 57

5000 85

T T T 28.20 28.40 28.60 28.80 113

m/z-> 0- puup 3! 141 169 197 225 253 1 Trn 11 nip 1 rq > n 11ri S24 324 ।n11 u 1111 > 1 ] Fgrr 20 40 60 80 100120140160180 200 220 240260280 300320 m/z 71.10 57.20%

Abundance #228992: Eicosane 57

5000 85 28.20 28*40 28.60 28.80 m/z 43.15 42.94% 29

0 1.... ’21’1 , ,.1 I i i I113 0111111111111122111117117 141. 169 282 ‘I‘10091731277T111111EETTTET""1‘1A19111112T m/z-> 20 40 60 80 100120140160180 200 220 240260280 300 320 Abundance #154905: Hexadecane 57

28.20 28*40 28.60 28.80 m/z 85.10 40.08% 5000 85 29 1 , 0-11021111 i 1.113 141 169 197 226.................. m/z-> 20 40 60 80 100120140160180200220240260280 300320 Abundance #245745: Heneicosane $$ n-Heneicosane ------ 57 28.20 28.40 28*60 28*80 m/z 55.10 20.34%

85 5000

29 1 113 141.169 197 225253... 298.... wM— wnpA

m/z—> 0 MHHM 20 40 60 80 100120140160180200220240260280 300 320 28'20 28.40 28.60 28.80

7110.D 5080402BBC.M Tue Apr 23 15:52:19 2002 Page 13

NYC-WTC_000049052

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NYC-WTC_000049052Source: NYC Law Department, mirrored locally

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