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GCMS sample AE07115 results, April 25, 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis results for sample AE07115 including detection of unknown compounds.

NYC-WTC_000049063–000049101

Folder label: “GCMS X 4/12/02 A 4/23/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\041002\7115.D Vial: 22 Acq On : 11 Apr 2002 7:15 am Operator: Bohik Sample : SAMPLE 7115 3/27/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 9 Eicosane Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

29.50 68.70 ug/L 8411860 Chrysene-dl2 30.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Eicosane 282 C20H42 000112-95-8 91 2 Nonadecane (CAS) $$ n-Nonadecane 268 C19H40 000629-92-5 91 3 Docosane $$ n-Docosane $$ Normal... 310 C22H46 000629-97-0 91 4 Octacosane (CAS) $$ n-Octacosane 394 C28H58 000630-02-4 91 Abundance Scan 4496 (29.496 min): 7115.D (-) m/z 57.10 100.00% 57

5000 85 —/----- --- — 1* 14*14** 1 ( Bs"""T"I‘l 1" 29.20 29.40 29.60 29.80 0-T a4.4.A.4134141,188,197,225,,253.281..309,33%. m/z 71.10 56.53% /z—> 20 40 60 80 100 120140160 180 200 220240 260 280 300 320 340 Abundance #228992: Eicosane 57

5000 85 29.20 29.40 29.60 29.80 m/z 43.20 41.98% 29

m/z—> 0 | HIM 141 169 Tgunp"n)"mROmapt 282 20 40 60 80 100120140160180200220240 260280 300 320340 Abundance #211483: Nonadecane (CAS) SS n-Nonadecane 57 —----- 29.20 29.40 29.60 29.80 m/z 85 15 39.67% 5000 85

0 ..... 11, 113, 141 169 197 225... 268.......... /z—> 20 40 60 80 100120140160180200220240260280300320340 Abundance #261311: Docosane $$ n-Docosane $$ Normal-docosane 57 29.20 29.40 29.60 29.80 m/z 55.10 21.08% 85 5000

_ _ - ■. I ., - J 3 1 1113 .4 0 urdl#4he . 1, .. J ■ 1169 197.225 253 281.. 310.... TTpoemmea—u*pnmgp—eape*g*monju /z—> 20 40 60 80 100120140160180200220240260280300320340 29*20 29.40 29.60 29.80

7115.D 5080402BBC.M Tue Apr 23 15:52:58 2002 Page 12

NYC-WTC_000049089

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NYC-WTC_000049089Source: NYC Law Department, mirrored locally

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