GCMS pesticide analysis results, sample AE11573, May-June 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\052902\11311RR.D Vial: 16 . Acq On : 29 May 2002 2:39 pm Operator: Bohlk / Inst 213 Sample : SAMPLE 11311 RE-EXTD 5/23/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\052802.M (RTE Integrator) 2** Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L *‘e-

Peak Number 3 Eicosane (CAS) $$ n-Eicosane Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

14.75 0.08 ug/L 118295 Acenaphthene-diO 18.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Eicosane (CAS) $$ n-Eicosane 282 C20H42 000112-95-8 90 2 Hexadecane 226 C16H34 000544-76-3 90 3 Docosane $$ n-Docosane $$ Normal... 310 C22H46 000629-97-0 90 4 Tridecane, 1-iodo- $$ Tridecyl i 310 C13H27I 035599-77-0 86 Abundance Scan 405 (14.749 min): 11311RR.D (-) m/z 71.10 100.00% 71

5000

99 <> i ■ ■ AALAAA Tl/Z-> 01 ml 49 11177 155.... 21......... I.) .. 1. ।. t. ।... 1).... ।.. ■. j.... । .. 11,..., ।.. I . ।., ,, ।.... । 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 14.40 14.60 14.80 15.00 m/z 57.10 94.29%

Abundance #228991: Eicosane (CAS) $$ n-Eicosane 57

5000 85 N A/..MA.N 14.40 14.60 14.80 15.00 m/z 85.10 71.68%

n/z-> ol m##=t 29 MX-—HL#„””+Z25. 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #154904: Hexadecane 57

_AA 14.40 14.60 14.80 15.00'71 5000 m/z 69.10 23.02% 85

29 ... 1 113 141 169 197 226 0! mpnt n/z-> Abundance 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 #261311: Docosane $$ n-Docosane $$ Normal-docosane 57 ' I 1 ' ' ■ I AA.M .1 .. 1 .1 . . I fl. 14.40 14.60 14.80 15.00 m/z 55.10 20.81% 85 5000

m/z—> 0, ml A111,162,,107225,253,201,,310, 20 40 60 80 100120 140 160 180 200 220 240 260 280 300 -AAAAALLI 14.40 14.60 14.80 15.00

1311RR.D 052802.M Mon Jun 03 15:50:17 2002 Page 5

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