GCMS pesticide analysis results, sample AE11573, May-June 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data* File : C:\MSDCHEM\l\DATA\052902\11311RR.D Vial: 16 . Acq On : 29 May 2002 2:39 pm Operator: Bohlk / Inst 213 Sample : SAMPLE 11311 RE-EXTD 5/23/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\052802.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L *‘**

Peak Number 2 Decane, 2,5,6-trimethyl- Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

11.59 0.06 ug/L 80114 Acenaphthene-dl0 18.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual l Decane, 2,5,6-trimethyl- 184 C13H28 062108-23-0 72 2 Nonane, 4,5-dimethyl- $$ 4,5-Dim... 156 C11H24 017302-23-7 64 3 Nonane, 4,5-dimethyl- (CAS) $$ 4... 156 C11H24 017302-23-7 64 4 2-Ethyl-1-dodecanol 214 C14H30O 019780-33-7 53 Abundance Scan 57 (11.593 min): 11311RR.D (-) m/z 57.10 100.00% 57 71 5000 85

98 *11.20AMwA... n/z-> 01 -48 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 "777.. m/z 11.40 11*60 11.80 12.00 71.10 64.26%

Abundance #93445: Decane, 2,5,6-trimethyl- 57 43

5000 N.M. 11.20 11.40 11.60 11.80 12.00 m/z 85.10 41.18% 71 84 98

n/z-> Of .। । ।. mm n i,.,127 r . । A I (.. n , ., । A 111 ■ I P| 111. ।113 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 1. j... 1111 I150 YY I 111 ■ >

Abundance #56268: Nonane, 4,5-dimethyl- $$ 4,5-Dimethylnonane 43 57

71 A Ar u N 11.20 11.40 11.60 11.80 12.00 m/z 84.10 37.53% 5000 85

0 29

20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #56269: Nonane, 4,5-dimethyl- (CAS) $$ 4,5-DIMETHYL-NONANE... 43 57 MMMort 11.20 11.40 11.60 11.80 12.00 m/z 55.00 37.15% 71 1 5000' 85

29 99 113 127

m/z—> 0 I I U I I I I rl .. I' TV + h +dpkmmmmmmmmmmm 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 ‘‘10T 11.20 11.40 11.60 11.80 12.00

1311RR.D 052802.M Mon Jun 03 15:50:16 2002 Page 4

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