GCMS pesticide analysis results, sample AE11573, May-June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052902\11311RR.D Vial: 16 Acq On : 29 May 2002 2:39 pm Operator: Bohlk / Inst 213 Sample : SAMPLE 11311 RE-EXTD 5/23/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1\5973N\052802.M (RTE Integrator) Title : Quantitation For Method 525.2 *‘** Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Undecane, 4,6-dimethyl- Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 11.48 0.05 ug/L 75183 Acenaphthene-dlO 18.19 Hit# of 5 Tentative ID MW MolForm CAS# Qual l Undecane, 4,6-dimethyl- 184 C13H28 017312-82-2 72 2 Dodecane, 2,6,11-trimethyl- $$ 2... 212 C15H32 031295-56-4 64 3 Dodecane, 2,6,10-trimethyl- $$ F. .. 212 C15H32 003891-98-3 64 4 Dodecane, 4,6-dimethyl- 198 C14H30 061141-72-8 56 Abundance Scan 44 (11.475 mln): 11311RR.D (-) m/z 71.10 100.00% 71 57

5000' 85

917.......... . 113 127 AMM. 11.20 11.40 11.60 11.80 0- ■ i ■ •' ■ i • •i m/z 57.00 79.10% i ■ ' 1 ■ i miz-> 20 40 60 80 100 120 140 160 180 200 Abundance #93418: Undecane, 4,6-dimethyl- 57 43

5000 71 WAAALA 11.20 11.40 11.60 11.80 m/z 85.20 42.38% 29 85 ..... all 98 113 0- ■ i •J■ • • i' ■,T Ai Mi ■ h..P./ 155 141 184 ■ ■ i •'i ■ i ■ • ‘ • i ■ ’ /z-> 20 40 60 80 100 120 140 160 180 200 Abundance #134042: Dodecane, 2,6,11-trimethyl- $$ 2,6,11-Trimethyldo... 57 43 71 -AAA 11.20 11.40 11.60 11.80 5000 m/z 84.10 26.63%

w Au 85 29 0- - . ■ A . , 4 . ”, 113,127 141 155 169,182 . miz-> 20 40 60 80 100 120 140 160 180 200 Abundance #134038: Dodecane, 2,6,10-trimethyl- $$ Famesan $$ Fames... 57 11.20 1140 11.60 1180 71 m/z 70.20 26.51%

5000 43

29 85

m/z—> ol 4 ,4 . , H , M , .4.7141.15 20 40 60 I

80 99 113 127 ..

100 120 140 =

160 183 197 180 200 1,. 11.20 11.40 11.60 11.80

1311RR.D 052802.M Mon Jun 03 15:50:15 2002 Page 3

NYC-WTC_000012621