GCMS sample results AE11284, DEP Labs, June 2002

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Data File : C:\MSDCHEM\1\DATA\020516\11284.D Vial: 12 Acq On : 16 May 2002 8:14 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integratof) Title : Method 508 GC/MS Scan Library : C: \DATABASE\nist98.1 ********************************************************************* Peak Number 2 0 Decane, 2,3,8-trimethyl- Concentration Rank 17 R.T. EstConc Area Relative to ISTD R.T. 22.74 0.64 ug/1 46823 Acenaphthene-dl0 24.46 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Decane, 2,3,8-trimethyl- 184 C13H28 062238-14-6 35 2 Undecane 156 C11H24 001120-21-4 27 3 Undecane, 3,8-dimethyl- 184 C13H28 017301-30-3 22 4 1-Decanol, 2,2-dimethyl- 186 C12H260 002370-15-2 14 Abundance Scan 3347 (22.745 min): 11284.D (-3330) (-) m/z 57.10 100.00% 43 57 156 141 71 5000 85 115 127 214111/04 MnAosA,4h, 22.40 22.60 22.80 23.00 niz-> U..,...-.... m .II —4 ■ ■ । ■ ■1 ■' i •' ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i •1111 >1111 • ■ 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11 ■1 rn/z 156.10 93.24% Abundance #16524: Decane, 2,3,8-trimethyl- 57 43 71

5000 85 .—7 22.40 22.60 22.80 23.00 29 111 m/z43.10 84.41% 99 141

miz-> —2l 1’’501’ 4TTT 20 30 40 I - 60 70 80 90 100 110 120 130 140 150 160 Abundance #112395: Undecane 43 57 ImpmodukaZyadtdbaad 22.40 22.60 22.80 23.00 5000 71 m/z 141.10 70.70% 85 29

niz-> 4 20 30 40 50 60 70 .1 Trr . | ila . 1 . . . 80 99 . . . . |113 1?7 I'l . . | , .‘I | 90 100 110 120 130 140 150 160 156 . 1 . . I I | ! I II | I I |

Abundance #16449: Undecane, 3,8-dimethyl- 43 57 22.40 22.60 22.80 23.00 71 m/z 71.10 60.54% 5000 85 29

TTr — M + 99 113 127 141 155 /z—> +21.4 li I'll I | . . > . । .. ’r > 1 | i i Ji j , i i . pl 1 I ■ | I l'l I | I |

20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 22.40 22.60 22.80 23.00

11284.D SCAN020507.M Fri May 17 13:06:54 2002 Page 23

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