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GCMS chain of custody form, sample AE10240, May 2002

Machine-extracted title · confidence 100%

Chain of custody record for GCMS analysis of sample AE10240 on May 20, 2002, including surrogate compound data.

NYC-WTC_000024390–000024401

Folder label: “GCMS X 5/1/02 A 5/9/02

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Scanned page image, NYC-WTC_000024398
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020509\10240.D Vial: 18 Acq On : 10 May 2002 3:25 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 1,6-Dioxacyclododecane-7,12... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

24.61 0.46 ug/1 62200 Acenaphthene-dl0 24.46

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,6-Dioxacyclododecane-7, 12-dione 200 C1OH1604 000777-95-7 43 2 6-Tridecanol 200 C13H280 005770-03-6 33 3 2-Eth acrolein 84 C5H8O 000922-63-4 27 4 2-Hex e, (E)-____________________________ 84 C6H12 004050-45-7 22 Abundance / Scan 3664 (24.607 min): 10240.D (-3657) (-) m/z 55.10 100.00% / 55

5000 84 - 41 100 111

pulphosjelngonam L 1141 129 24.20 24.40 24.60 24.80 25.00

mfz-> mmmmH 69 । 156 182 ’’1’1 1 ‘I'1 “I 1,1 'i" " i11" i11" r "11" ■ ‘ i 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 m/ Z 84.05 31.60% Abundance #13624:1,6-Dioxacyclododecane-7,12-dione 55

5000 27 41 84 MWMMW MMw 24.20 24.40 24.60 24.80 25.00 100 71 129 m/z 111.10 20.50% 15 1111 | 141 152 172182 200 - parl— I 1140 11 I Nommmmm—p miz- > 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #13929:6-Tridecanol 55 60 41 83 .AA 1... A... 24.20 24.40 24.60 24.80 25.00 5000 m/z 56.10 19.73% 29 101111 129 182 4 +— TIT 154 | mmmmm

.... A......... ■ i ■ ■" I"' ■ i ■"' i1" ■ i'' ■' r m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #14365:2-Ethylacrolein 55 24.20 24.40 24.60 24.80 25.00 84 m/z 100.10 19.19%

5000 29 39 _

69 THT] ‘TTpT-rrpTTT7TTTTTrrTTpTTTpTTTpTTTTTTTTp^ m/z—> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 24.20 24.40 24.60 24.80 25.00

10240.D SCAN020507.M Tue May 14 14:25:23 2002 Page 5

NYC-WTC_000024398

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NYC-WTC_000024398Source: NYC Law Department, mirrored locally

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