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GCMS analysis results for sample AE10246, May 28, 2002

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Laboratory report documenting GCMS analysis of sample AE10246 conducted on May 28, 2002, including surrogate recovery data.

NYC-WTC_000024883–000024895

Folder label: “GCMS X 5/14/02 A 5/17/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020509\10246.D Vial: 24 Acq On : 10 May 2002 9:21 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 6 Z-1,6-Tridecadiene Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 36.88 0.43 ug/1 47883 Chrysene-dl2 39.93 Hit# of 5 Tentative ID MW MolForm CAS# Qual

— 1 Z-1, 6-Tridecadiene 180 C13H24 1000130-98-3 80 2 2 loroethyl linoleate 342 C20H35C1O2 025525-76-2 68 3 trans-Bicyclo [5.1.0] octane 110 C8H14 021370-66-1 64 4 5-Nonadecen-1-01 282 C19H380 1000131-11-9 59 Abundant Scan 5753 (36.881 min): 10246.D (-5742) (-) m/z 67.20 100.00% 67 82 41 5000 109 M A AMA/ miz-> 40 60 II III | 124 155

80 100 120 140 160 180 200 220 240 260 280 300 320 340 281 36.60 36.80 37.00 37.20 m/z 81.10 85.90% Abundance #13102: Z-1,6-Tridecadiene 55 41 82 5000 I AAd , ...... 36.60 36.80 37.00 37.20 109 m/ z 82.10 74.01%

TTI — r M I I , 124,152 180 r " ' 1 "al "I ' ' 1 ' 1 1 t | I I I I I I I I I I I IJI > | I I I I I 1-p I I I I I I 1 1 | I I I I I I I n/z-> 40 60 80 100 120 140 160 180 200 220 .240 260 280 300 320 340 Abundance #21410:2-Chloroethyl linoleate 67 A.B, al I,, "hmMha, 36.60 36.80 37.00 37.20 95 m/ z 41.20 62.31% 5000 N 41 109 — II # J —4+—’135150 263 342 A ! 11 i r1122‘‘1‘10111111011110‘70101110‘111033111-T m/z— > Abundance 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340

41 67 #21071: trans-Bicyclo[5.1 .OJoctane uasuesdbadM“Ww 36.60 36.80 37.00 37.20

.A 82 m/z 55.10 61.95%

5000

110 ‘‘1‘211110011111101101111111511111001000-mm —nummg A 11" 111' m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 36.60 36.80 37.00 37.20

10246.D SCAN020507.M Tue May 14 14:26:41 2002 Page 8

NYC-WTC_000024892

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NYC-WTC_000024892Source: NYC Law Department, mirrored locally

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