GCMS analysis report sample AE10245, May 2002

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Data File : C:\MSDCHEM\1\DATA\020516\10245.D Vial: 21 Acq On : 17 May 2002 5:06 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 5 2-Propenoic acid, n-pentade... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 38.54 0.43 ug/1 26249 Chrysene-dl2 39.93 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propenoic acid, n-pentadecyl e... 282 C18H34O2 1000245-64-0 59 2 2-Propenoic acid, n-tridecyl ester 254 C16H30O2 1000245-63-8 56 3 1-Dodecanol, 3,7,11-trimethyl- 228 C15H320 006750-34-1 40 4 5-Octadecene, (E) -_______________________ 252 C18H36 007206-21-5 38 Abundance Scan 6035 (38.538 min): 10245.D (-6028) (-) m/ z 55.10 100.00% 55

83 43 73 5000 97 AA A AA AAA 1-1 I1 ' 1 1 1 ' 1 11■ । ■ 1 ' 'i 111 127 38.20 38.40 38.60 38.80 11" " i"11 [ " r I i pt Iil ....... 1.......... 1 ।।■ i ■ > ■ ■।■ l1' ■ ■।■>■> । ■ ■ ■>।«1 > i ■ • • > I" " I" >> I >" ‘ I m/z 83.20 70.57% m/z-> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #13489:2-Propenoic acid, n-pentadecyl ester 55

5000 43 A,A I, H Ah .A 73 83 38.20 38.40 38.60 38.80 97 m/ z 43.10 61.52% 111 127

/z—> ft 41ll-7l+139...153.,166,.182.77210.. 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #13488:2-Propenoic acid, n-tridecyl ester 55 Alatashpalaadada,4halaA 38.20 38.40 38.60 38.80____ 5000 43 m/z 73.10 51.20% 73 83 97 111 127

n/z-> ........ ... +64444—— j 139 154 THTTTTTT 182

Abundance :20 30 40 50 60 70 80 90 100110120130140150160170180190200210 #111538:1 -Dodecanol, 3,7,11 -trimethyl- k...... 1 1 I 1 1 ' 1 I 1 1 A......... I ' ■ ■ ' I ' ' ‘ ' I 43 55 69 38.20 38.40 38.60 38.80 m/z 57.20 48.44% 83 5000 97 111 125 ++ 29

/z—> TT I... ||.... Il... 1140............................ ‘ 1 r 11 1 1 ' " 1 I" ' I | J ri 1 | I t ! | [ t 1 > I | I I I | | ) ! > ! | J I | | | m t [ ! | | | | | | | ! | | ( J J | 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 —A44... 4 38.20 38.40 38.60 38.80

10245.D SCAN020507.M Fri May 17 10:46:35 2002 Page 7

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