GCMS analysis results for sample AE11158, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020515\11158.D Vial: 10 Acq On : 15 May 2002 8:43 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 7 Pentadecane, 2,6,10-trimethyl- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 43.28 0.90 ug/1 51916 Perylene-dl2 43.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pentadecane, 2,6,10-trimethyl- 254 C18H38 003892-00-0 50 n 2 Hexadecane 226 C16H34 000544-76-3 50 3 Dodecane, 2,7,10-trimethyl- 212 C15H32 074645-98-0 50 4 Hexadecane, 7-methyl- 240 C17H36 026730-20-1 50 Abundance Scan 6842 (43.280 min): 11158.D (-6837) (-) m/z 57.10 100.00% 57 71 5000 43 85 97 14nan 4 .4 , w w II ■ ■ i 1 ■1 ■ i Hal..1111182147 ..... 191 216.232 261 । । II । । I < । । । । i > 7 । ■ r I > । । i I I | I | I I | | | | i | | I I r । i I I I | | । m/z 43.00 43.20 43.40 43.60 71.20 75.79% m/z->20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #16428: Pentadecane, 2,6,10-trimethyl- 57

43 5000 71 kA,, A,A AMAAw A #AA 43,00 43.20 43.40 43.60 85 m/z 43.10 38.28% 99 111 , II. i .d 13 127 141 155 169 183 197211 225 239 254 tt i 1 11 ‘ i1 11 1 1 1 ■1 ■ i ’ ’ ■ ■ I ' 1 I '' 1 1 | ' । । । । । । । । । । । । । । । । । > j । । n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #112409: Hexadecane 43 57 71 nAkwrhun AA "hAntushpr 43.00 43.20 43.40 43.60 5000 85 m/z 85.05 31.41% 99 A 29 , 15 | 1.1 . | . , 127 141 155 169 183 197 211 226.......... 1 ■ ' ■ i ■ ■' TTT TT" 1 1 1 11 ' 1 I ' ' 1 ' I 11 ' ' r ' • ' ' | 1 l , | I 'I 1-1 r I | 1 I I | III I I I I | I 1 | I I m/z-> Abundance 20 40 60

57 80 100 120 140 160 180 200 220 240 260 #17104: Dodecane, 2,7,10-trimethyl- Un kal w.lnall Aallla, 43.00 43.20 43.40 43.60 71 m/z44.00 19.90% 43 5000

29 85 , J. 99 113 127 141 155 169 1 83 197______________ ■" i' 1,' r— I, i * I1 ' । ' ' 'i' ' ’’ i ’ '' i ' ' '1 i ' ' ' ■ i ■ ■ ' ■ i ■ 1 1 ' i ■ ' ■ ■ i 1 ■ ■ ■ i ' ■ n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 43.00 43.20 43.40 43.60

11158.D SCAN020507.M Thu May 16 09:53:08 2002 Page 9

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