GCMS sample results AE11284, DEP Labs, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020516\11284.D Vial: 12 Acq On : 16 May 2002 8:14 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 17 Pentadecane Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 17.26 1.09 ug/1 78047 Naphthalene-d8 16.53 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Pentadecane 212 C15H32 000629-62-9 72 2 Dodecane 170 C12H26 000112-40-3 72 3 Dodecane 170 C12H26 000112-40-3 64 4 Eicosane 282 C20H42 000112-95-8 59 Abundance Scan 2413 (17.257 min): 11284.D (-2399) (-) m/z 57.10 100.00% 43 57

5000 71 85

99 170 17.00 17.20 17.40 17.60 11 ■ • i ■ • 1 ‘ i ■ • "1 ■ 'I111' » l hi ■ rJ * * • * I ‘ ‘ 136 ‘ ‘ I ’ ‘ * 'I « » I » I I I » J I I » » • I m/z 43.05 88.09% mfz-> 20 40 60 80 100 120 140 160 180 200 Abundance #112369: Pentadecane 57 43

5000] 71 85 17.00 17.20 17.40 17.60

nz-> Abundance a 20 +■ 40। 60 43 57 QQ 7 113 127 141 155 168 182 212 T 1 ■ 1a, । • i * 1 ‘“r • • • • i * • • i * * • • । • ' * • । ’ • । ■ i 80 100 120 140 160 180 200 #109555: Dodecane m/z 41.10 43.02%

a“bsckabmyheKAmy"sdtuAA 17.00 17.20 17.40 17.60 5000 29 71 m/z 71.10 41.13% 85 . . ■ P ' ■"! , 99 113 127 141 170 MU . । ’l". . . । . । r . । । . । > > . ■ । । । । i । । । n/z-> Abundance 20 40 60 I80 100 120 140 #112317: Dodecane 160 180 200 i MAA.rAA.AM1 1411 AAAf A 43 57 17.00 17.20 17.40 17.60 m/z 85.20 34.50% 71 5000 85 29

mz—> . 15, 20 ll., 60-4 40 * 112127 . l 141 155 170‘I*‘ tTss1+sFI** 80 100 120 140 160 180 200 .... I*IT+‘II ,A-A4,444uluk 17.00 17.20 17.40 17.60

11284.D SCAN020507.M Fri May 17 13:06:48 2002 Page 20

NYC-WTC_000014802