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Document / 12 pages

GCMS sample AE11154 analysis with surrogate recovery, May 2002

Machine-extracted title · confidence 90%

GCMS analysis page for sample AE11154 showing unknown compounds and surrogate compound recovery data.

NYC-WTC_000025556–000025567

Folder label: “GCMS X 5/17/02 A 5/16/02

Page image
Scanned page image, NYC-WTC_000025556
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\MSDCHEM\l\DATA\020515\11154.D Vial: 20 Acq On : 16 May 2002 6:34 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 16 08:41:38 2002 Quant Results File: SCAN020507.RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Wed May 15 15:22:39 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.37 152 430425 40.00 ug/1 -0.02 10) Naphthalene-d8 16.53 136 1604812 40.00 ug/1 -0.04 17) Acenaphthene-diO 24.45 164 860670 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.72 188 1480009 40.00 ug/1 -0.02 38) Chrysene-dl2 39.93 240 1198518 40.00 ug/1 -0.05 44) Perylene-dl2 43.15 264 717082 40.00 ug/1 -0.03

System Monitoring Compounds 27) TCMX 27.55 207 226626 3296/ug/1 . 02 Spiked Amount 40.000 Recovery = ( 82.40%

Target Compounds \ Ovalue 35) Di-n-butylphthalate 34.80 149 9027 0.19 ug/l 95 43) Bis(2-ethylhexyl)phthalate 40.52 149 155316 6.05 ug/I 99

(#) = qualifier out of range (m) = manual integration (+) = signals summed 11154.D SCAN020507.M Thu May 16 09:33:16 2002 Page 1

NYC-WTC_000025556

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NYC-WTC_000025556Source: NYC Law Department, mirrored locally

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