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← Document results/DEP Box 18/GCMS X 5/13/02 A 5/15/02
Document / 13 pages

GCMS analysis results, sample AE11157, May 22, 2002

Machine-extracted title · confidence 80%

GCMS analysis for sample AE11157 identifying other unknown compounds with a 2,4-DDD surrogate recovery of 91%, completed May 22, 2002.

NYC-WTC_000024652–000024664

Folder label: “GCMS X 5/13/02 A 5/15/02

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Scanned page image, NYC-WTC_000024654
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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\MSDCHEM\l\DATA\020515\11157.D Vial: 9 Acq On : 15 May 2002 7:43 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 16 09:37:25 2002 Quant Results File: SCAN020507 . RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Wed May 15 15:22:39 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) l,4-Dichlorobenzene-d4 11.38 152 444754 40.00 ug/1 -0.01 10) Naphthalene-d8 16.53 136 1687299 40.00 ug/1 -0.04 17) Acenaphthene-diO 24.46 164 914736 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.72 188 1560740 40.00 ug/1 -0.02 38) Chrysene-dl2 39.93 240 1284779 40.00 ug/1 -0.05 44) Perylene-dl2 43.15 264 771868 40.00 ug/1 -0.03

System Monitoring Compounds 2 7) TCMX 27.55 207 266130 36.42 ug/1 -0.02 Spiked Amount 40.000 Recovery 91.05% Target Compounds Qvalue 35) Di-n-butylphthalate 34.80 149 8050 0.16 ug/1 92 43) Bis(2-ethylhexyl)phthalate 40.52 149 41978 1.53 ug/1 96

(#) = qualifier out of range (m) = manual integration (+) = signals summed 11157.D SCAN020507.M Thu May 16 09:38:36 2002 Page 1

NYC-WTC_000024654

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NYC-WTC_000024654Source: NYC Law Department, mirrored locally

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