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GCMS analysis results for sample AE10246, May 28, 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AE10246 conducted on May 28, 2002, including surrogate recovery data.

NYC-WTC_000024883–000024895

Folder label: “GCMS X 5/14/02 A 5/17/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\MSDCHEM\1\DATA\020509\10246.D Vial: 24 Acq On : 10 May 2002 9:21 am Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 14 14:17:38 2002 Quant Results File: SCAN020507.RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) W / Title : Method 508 GC/MS Scan X V y Last Update : Thu May 09 09:21:01 2002 W N Response via : Initial Calibration y DataAcq Meth : 508SCAN1 V

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.37 152 523309 40.00 ug/1 -0.02 10) Naphthalene-d8 16.53 136 1983002 40.00 ug/1 -0.04 17) Acenaphthene-diO 24.46 164 1065797 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.72 188 1805230 40.00 ug/1 -0.02 38) Chrysene-dl2 39.93 240 1440756 40.00 ug/1 -0.05 44) Perylene-dl2 43.15 264 922467 40.00 ug/1 -0.03

System Monitoring Compounds 27) TCMX 27.53 207 51549 6.05 ug/1 -0.04 Spiked Amount 10.000 Recovery = 60.50% Target Compounds Qvalue 43) Bis(2-ethylhexyl)phthalate 40.52 149 4783 0.15 ug/1 86

(#) = qualifier out of range (m) = manual integration (+) = signals summed 10246.D SCAN020507.M Tue May 14 14:18:50 2002 Page 1

NYC-WTC_000024883

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NYC-WTC_000024883Source: NYC Law Department, mirrored locally

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