GCMS analysis results, sample AE10135, May 2002

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\l\DATA\020513\10135.D Vial: 21 Acq On : 14 May 2002 8:22 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 15 08:29:00 2002 Quant Results File: SCAN020507.RE

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Thu May 09 09:21:01 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.37 152 459473 40.00 ug/1 -0.02 10) Naphthalene-d8 16.53 136 1711925 40.00 ug/1 -0.04 17) Acenaphthene-diO 24.46 164 910381 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.72 188 1565444 40.00 ug/1 -0.02 38) Chrysene-dl 2 39.94 240 1257209 40.00 ug/1 -0.05 44) Perylene-dl2 43.15 264 763487 40.00 ug/1 -0.03

System Monitoring Compounds 27) TCMX 27.54 207 70021 9.63 ug/1 -0.04 Spiked Amount 10.000 Recovery = 96.30%

Target Compounds Qvalue 43) Bis(2-ethylhexyl)phthalate 40.52 149 14062 0.52 ug/1 91

(#) = qualifier out of range (m) = manual integration (+) = signals summed 10135.D SCAN020507 .M Wed May 15 08:30:15 2002 Page 1

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