GCMS sample results AE11284, DEP Labs, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020516\11284.D Vial: 12 Acq On : 16 May 2002 8:14 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) ** Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 16 2H-Inden-2-one, 1,3-dihydro- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 15.93 0.97 ug/1 69272 Naphthalene-d8 16.53 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2H-Inden-2-one, 1,3-dihydro- 132 C9H80 000615-13-4 43 2 Indan,/epoxide 132 C9H80 000768-22-9 41 3 2H-Inden-2-one, 1,3-dihydro- 132 C9H80 000615-13-4 41 4 Naphthalene, 1,2,3,4-tetrahydro- 132 C10H12 000119-64-2 35 Abundance f Scan 2187 (15.929 min): 11284.D (-2171) (-) m/z 119.10 100.00%| 104 1‘ 9 91

5000 71 78 132 A. 43 51 58 148

mtz-> 20 — 44 I I ll IL 30 40 50 60 70 I ‘ ‘ 80 ’ I * 90 4 100 110 120 130 140 150 15.60 15.80 16.00 16.20 m/z 104.20 88.17% Abundance #118898: 2H-Inden-2-one, 1,3-dihydro- 104

» .......... .................... 5000 78 132 15.60 15.80 16.00 16.20 ' ' 1 51 m/z 105.10 78.40% 39 63 ■ ■ l ■ pl । ■■

niz-> 20 -HH ■ al 30 40 50 60 70 80 90 100 110 120 130 140 150 89 ■ • i • • ■ ■ i1' • • i 1 ■ i ■ ■1 ■ i ■ ■

Abundance #45085: Indan, epoxide 104 LAA4AADAA 15.60 15.80 16,00 16.20 5000 m/z91.00 75.98% 51 78 132

mz-> Abundance ‘tI.T 20 127 39 11) 111 rl till

30 40 50 63 i 89 • ’i ■ TH+ 60 70 80 90 100 110 120 130 140 150 #118980:2H-inden-2-one, 1,3-dihydro- 104 4 1 ■ i ■ ■ ■ • i ■ • _AAAA 15.60 15.80 16.00 16.20 m/z 132.00 28.20% 5000 78 132 51 39 27 । .3 70.1,8997 89 97 1 115 TIT hgrerlpoans I I 1 1/20n0/t—I I J 14 Illi k k' i •1 •11 * • • • i TT-p-TT-T-p-T ’-14**I4*/"’+’I4IIE /z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 15.60 15.80 16.00 16.20

11284.D SCAN020507.M Fri May 17 13:06:46 2002 Page 19

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