Laboratory report of GCMS analysis for sample AE10244 conducted on May 28, 2002.
NYC-WTC_000024832–000024842Folder label: “GCMS X 5/14/02 A 5/17/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020516\10244.D Vial: 20 Acq On : 17 May 2002 4:07 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 2-Propen-1-one, 1-(2-hydrox... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 31.10 0.25 ug/1 20836 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Propen-1-one, 1-(2-hydroxy-3-m.. 192 C11H12O3 040992-03-8 50 2 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 47 3 Bitoscanate 192 C8H4N2S2 004044-65-9 47 4 Bitpscanate 192 C8H4N2S2 004044-65-9 47 Abundance Scan 4769 (31.100 min): 10244.D (-4758) (-) m/z 192.10 100.00% 192
5000
96 146 160 49 64 84 TTTTTTTTHT q mr) poolapo 30.80 31.00 31.20 31.40 m/ z 96.00 23.36% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80998:2-Propen-1-one, 1-(2-hydroxy-3-methoxy-6-methylphe... 192
165 177 ■’“'I 1 1 1 1 1 1 1 5000 131 ' i ' ■ ' ' i ' ' 30.80 31.00 31.20 31.40 55 65 77 103 121 m/z 191.00 18.68%
n/z-> 4 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 1___ 1" I'1
Abundance #80950:1,5-Naphthalenedithiole 192
30.80 31.00 31.20 31.40 5000 m/z 194.00 17.53% 115 128 159
40 57• 69 79 96 . 147 177 11"'11h1 r*111111------hr — ■ r । ■ TTp-r m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80930: Bitoscanate ' 1 1 11 1 1 1 1 1 1 I ‘ 1 1 ' I ' ' 192 30.80 31.00 31.20 31.40 m/z 160.10 15.87% 5000 134 90 160 63 75
/z—> +26,39. 4 i 107 116 TTTTTTHT 148 1 r " 11" " i 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 .........1’1’ 30.80 31.00 31.20 31.40 1 1 1 1 1 1 1 1 1
10244.D SCAN020507.M Fri May 17 10:44:36 2002 Page 5
NYC-WTC_000024840
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NYC-WTC_000024935
Chromatogram and integration data from Method 508 GC/MS analysis of sample AE10302 performed on May 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024851
GCMS analysis results for sample AE10245 conducted May 28, 2002, showing unknown compounds and 2,4-DDD surrogate recovery at 86 percent.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024871
Laboratory report of GCMS analysis for sample AE10246 conducted on May 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024896
Laboratory report of GCMS analysis for sample AE10247 conducted on May 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024813
Laboratory report of GCMS analysis for sample AE10243 conducted on May 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024390
Chain of custody record for GCMS analysis of sample AE10240 on May 20, 2002, including surrogate compound data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024915
Laboratory report of GCMS analysis for sample AE10301 conducted on May 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025613
GCMS analysis report for sample AE11571 showing unknown compounds and surrogate recovery data from May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024412
Chain of custody record for GCMS analysis of sample AE10238 on May 20, 2002, including surrogate compound data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025568
GCMS analysis report for sample AE11567 showing unknown compounds and surrogate recovery data from May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046159
Laboratory report listing GCMS results for unknown compounds and surrogates from sample AE10130 on May 17, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043806
Analytical report for sample AE09769 documenting GC/MS analysis of unknown compounds and surrogate recovery data from May 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000024743
Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
Filed in the same folder
NYC-WTC_000024744
Index or cover page for the GCMS document series covering samples from May 14 to May 17, 2002.
Filed in the same folder
NYC-WTC_000024748
Reference document describing Method 509 procedures for laboratory analysis, dated February 14, 1992.
Filed in the same folder
NYC-WTC_000024758
Laboratory report of a GCMS blank run for sample AE10241 conducted between May 14 and May 16, 2002.
Filed in the same folder
NYC-WTC_000024762
Laboratory report of GCMS calibration data for sample AE10241 conducted between May 14 and May 16, 2002.
Filed in the same folder