GCMS quantitation results for sample AE10244, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020516\10244 .D Vial: 20 Acq On : 17 May 2002 4:07 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 Anthracene-dlO- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

31.95 0.33 ug/1 26910 Phenanthrene-dl0 31.72

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 59 2 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 37 3 Benzaldehyde, 2,6-difluoro-4-hyd... 188 C8H6F2O3 1000116-28-9 28 4 Phenanthrene-diO__________________________ 188 C14D10 001517-22-2 10 Abundance / Scan 4913 (31.946 min): 10244.D (-4907) (-) m/z 188.15 100.00% 188

5000 94 49 66 80 160 170 31.60 31.80 32.00 32.20 - i" " i m/z 189.20 24.80% mz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 31.60 31.80 32.00 32.20 m/z 94.05 23.52% rr 80 94 160 , 17 30 42 52 0 . J 108118 132 146 1. 170179.1.1 I < । ■ i < । ■> I ■ | ■ I ■ > ] I i i i ] I ! i i p I I ■ । ■ I I I | I i i I | I I ■ i |~t I I I | I I I I | I I 1 I | I I ! I | 1 1 t I | I I “T’t I I r j i i i | | |'|rl I | I I I ‘i miz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #125696:2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime its .......................... ........................ , 31.60 31.80 32.00 32.20 5000 m/z 184.20 18.97% 143

mlz—> Abundance 'i""i""i 51 64 76 J 102 115 130 11111 i'i ii 11 ‘‘i r i'I'i 111 II| । ii 11 ii । pill 111 ir‘ 11111 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 #79823: Benzaldehyde, 2,6-difluoro-4-hydroxy-3-methoxy- . -HH 158 170 u 4. - । t I i । । r i i i । i

US 31.60 31.80 32.00 32.20 m/z 66.10 15.07% A 5000 173 43 57 69 78 88 97 106 117 2- -H L 145

n/z—> -------+--+++----+-4444 — lP9 —+ 128 + 155 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 ■ i" " i' | ' I T I 1 ' r ' I*r | I I I 1 | I I I I | 1

31.60 31.80 32.00 32.20

10244.D SCAN020507.M Fri May 17 10:44:37 2002 Page 6

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