GCMS results for sample AE11426, May 29, 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020521\11426.D Vial: 12 Acq On : 21 May 2002 7:14 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 Anthracene-dlO- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 31.96 0.32 ug/1 35711 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-dlO- 188 C14D10 001719-06-8 50 2 1,2-Bis(2-hydroxyphenyl)ethylene... 376 C24H28N2O2 1000187-13-2 42 3 Phenanthrene-diO 188 C14D10 001517-22-2 38 4 Nalidixic Acid 232 C12H12N2O3 000389-08-2 33 Abundance Scan 4916 (31.963 min): 11426.D (-4908) (-) m/z 188.15 100.00% 188

5000 80 ............................ ........... 40 132 156 । 245 31.60 31.80 32.00 32.20 0- TWTengT m/ z 80.10 28 .45% miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #79826: Anthracene-d10- 188

5000 31.60 31.80 32.00 32.20 m/z 189.20 24.20% __ 94 160 I

Ti/z-> 0 „17—42.—6641141324 ■ ‘ i1" ‘ i ‘ " i" " i'" ■ i11 ■ ■ i' “ ‘ i " 1 ■ i “ ■ ■ i" ■' i" 20 40 60 80 100120 140160180 200 220 240 260 280 300 320 340 360 380 Abundance #79831:1,2-Bis(2-hydroxyphenyl)ethylenediamine, N,N'-bis(... 188 .......... ................ ............ 31.60 31.80 32.00 32.20 5000 m/ z 94.00 15.67%

41 77 94 I Y | | 121 145 171 0 — .t PPM.+th rW ", 144). Ar err ■. 111Il I I |T .. | 210 238255 293 377 ’11 ■ {-1 i i 17 ■ i ri [ > ■ i > I i i i Tr i i i , I i i i ■ f r । i i j | I > i j | I z-> 20 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 ' I / y— । । । । ri i । । i Abundance #79827: Phenanthrene-d10 188 31.60 31.80 32.00 32.20 m/z 187.25 12.90% 5000

80 160

n/z-> 30 52 0 Ttt +190.132 4— A .......... I" '' I " " I " '11' " ' I " '' I' " ' 11111T" 111111111111111 ' i 1 ' ' 'T1 ' 1 1 | ' 1 1 1 1 1 1 1 1 1 1 20 40 60 80 100 120 140160180 200 220 240 260 280 300 320 340 360 380 31.60 31.80 32.00 32.20

11426.D SCAN020521.M Fri May 24 09:28:42 2002 Page 6

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