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GCMS analysis page for sample AE11568, May 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AE11568 showing unknown compounds and surrogate recovery data from May 29, 2002.

NYC-WTC_000025580–000025591

Folder label: “GCMS X 5/17/02 A 5/16/02

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Scanned page image, NYC-WTC_000025590
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\O2O521\11568 .D Vial: 21 Acq On : 22 May 2002 4:07 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 5 Anthracene-d10- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 31.95 0.38 ug/1 36390 Phenanthrene-dl0 31.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 53 2 Phenanthrene-diO 188 C14D10 001517-22-2 53 3 1,2-Bis(2-hydroxyphenyl)ethylene... 376 C24H28N2O2 1000187-13-2 50 4 1,4-^Japhthalenedione, 2-hydroxy- . . . 188 C11H8O3 000483-55-6 37 Abundance Scan 4914 (31.952 min): 11568.D (-4907) (-) m/z 188.10 100.00% 188

5000 92 160 52 132 H 31.60 31.80 32.00 32.20 0 ________ — H ihli 111 ‘111 rw 11111 i JI I ________________________________________ TI’1 1111‘01111110111111111111111071110111——I10B3701T m/z 92.10 29.67% n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #79826: Anthracene-d10- 188 ...................................................... 5000 31.60 31.80 32.00 32.20 m/z 189.20 24.67% rr 94 160 0 „17..442.46641,1141224 ’’I’’’’)’’)GHSET’hBNA*R3 m/z-> 20 40 60 80 100120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #79827: Phenanthrene-d10 188

31.60 31.80 32.00 32.20 5000 m/ z .94.20 20.56%

80 160 0 30 l ""I''- 52,144199.132— mlz-> 20 40 60 80 100120 140160 180 200 220 240 260 280 300 320 340 360 380 Abundance #79831:1,2-Bis(2-hydroxyphenyl)ethylenediamine, N,N'-bis(... 188 31.60 31.80 32.00 32.20 m/z 184.20 18.67% 5000

41 77 94 । 121 145 171 ..... .............. 0 -HPA--H , 210 238255 . I 293____________ 377 | . ri'[i 1 n 11 u 111 > 1111111111 ITi 111111 I I | I n/z-> 20 40 60 80 100120 140 160180 200 220 240 260 280 300 320 340 360 380 31.60 31.80 32.00 32.20 ___

11568.D SCAN020521.M Fri May 24 09:42:41 2002 Page 7

NYC-WTC_000025590

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NYC-WTC_000025590Source: NYC Law Department, mirrored locally

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