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GCMS analysis page for sample AE11568, May 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AE11568 showing unknown compounds and surrogate recovery data from May 29, 2002.

NYC-WTC_000025580–000025591

Folder label: “GCMS X 5/17/02 A 5/16/02

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Scanned page image, NYC-WTC_000025589
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020521\11568.D Vial: 21 Acq On : 22 May 2002 4:07 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 4 Pentamethylbenzoic acid Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 31.10 0.30 ug/1 29219 Phenanthrene-dl0 31.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pentamethylbenzoic acid 192 C12H1602 002243-32-5 47 2 Anthracene, tetradecahydro-, (4a... 192 C14H24 001755-19-7 47 3 Anthracene, tetradecahydro- 192 C14H24 006596-35-6 47 4 4-Isothiazolamine, 3,5-bis (methy. . . 192 C5H8N2S3 037572-42-2 32 Abundance 7 Scan 4769 (31.100 min): 11568.D (-4756) (-) ’ m/z 192.10 100.00% I 192

5000 146 160 ----- 51 122 | 252 30.80 31.00 31.20 31.40 01 i....................... Ill . , , 1 ' 1 ■ i 1 ' ■ ■ i ■ ■ ' ■ i 1 I ‘ ‘‘I* i ■ ■ — I • ]''*» l^' I J I l i• fI I I m/z 191.20 29.28% m/z-> 0 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #80979: Pentamethylbenzoic acid 131 147 174 1:2 A

5000 91 A.... r 1 1 11 ' 1 | 1 ’I’***I" 39 51 65 77 115 30.80 31.00 31.20 31.40 27 m/z 146.00 27.02% 159 0- TTr . । Li „l/,npla L 4, Il d4 unin ■ ■n/z-> 0 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #80932: Anthracene, tetradecahydro-, (4a.alpha.,8a.alpha.... 192 ) 135 30.80 31.00 31.20 31.40 5000 67 m/z 193.00 16.12%| 81 95 55 121 150

0 i ■ ' ' ■ i 1 ' 1.11,797, I .1, - 163 177 1 I ■ 1 ■ ■ i ■ 1 ■ ■ i ■ 1 ■ ‘ i nfe-> 0 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #80931: Anthracene, tetradecahydro- .....I I . 1 i ' 1 135 192 30.80 31.00 31.20 31.40 m/z 160.10 15.85% 67 81 95 5000 121 41 55 150

■nfz~> 0 —20 2d 0 144 40 60 80 100 120 140 163

160 177 180 ■ । ■' ■ ■ ।1111111111 200 220 240 30.80 31.00 31.20 31.40

11568.D SCAN020521.M Fri May 24 09:42:39 2002 Page 6

NYC-WTC_000025589

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NYC-WTC_000025589Source: NYC Law Department, mirrored locally

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