Method 509 reference document, February 1992

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020516\0514LB.D Vial: 5 Acq On : 16 May 2002 1:19 pm Operator: Nefliu Sample : 05/14 lab blk Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 Anthracene-dlO- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.96 0.29 ug/1 22631 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-diO- 188 C14D10 001719-06-8 64 2 Phenanthrene-d10 188 C14D10 001517-22-2 64 3 Pentacyclo[7.3.1.1.(4,12).0(2,7)... 188 C14H20 1000215-61-8 45 4 1-Naphthalenecarboxylic acid, 7-... 188 C11H803 002623-37-2 9 Abundand Scan 4915 (31.958 min): 0514LB.D (-4905) (-) m/z 188.20 100.00% 188

5000 80 94 158 40 54 31.60 31.80 32.00 32.20 qmmmmm*mmmmmmmmmmmmmmmmmmmmmmmmm m/ z 80.20 22.66% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 31.60 31.80 32.00 32.20 m/z 189.20 22.50% 80 94 160 । 17 30 42 52 ° . J 108118 132 146 I 1701791 1 । | । । 1 | i i i i | | | | । | I i n-| I I ii , lit 11 i i I I p i I 11 I I i i | I i i I । i । i I । i i । । । 11 | । । । । 1 । p i iTpi i [ i | i i i i | I’l’f V-rrT

n/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

31,60 31.80 32.00 32.20 5000 m/z 94.10 15.65%

80 94 160 30 42 52 66 , | 108118 132 146 . C TITTTTTTTTTTTTTTTTTTTTTTTTTHTTT 11 I 11 r| 11 11 11 । 11111 । "TH 111 11 111 i it 17917 . /z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79715: Pentacyclo[7.3.1.1 .(4,12).0(2,7).0(6,11)]tetradeca... IIfaaLTit TTT’I । । । । । i 188 31.60 31.80 32.00 32.20 m/z 158.10 11.71% 5000 79 91 55 67 1 117 131 105

1 aHuligaan 145.158/173.. II,.... 1Iu——BNUmtnn n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20

0514LB.D SCAN020507 ,M Fri May 17 10:36:12 2002 Page 6

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