GCMS analysis page for sample AE11568, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020521\11568.D Vial: 21 Acq On : 22 May 2002 4:07 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 3 DL-Anabasine Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 28.91 0.24 ug/1 23236 Phenanthrene-dl0 31.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 DL-Anabasine 162 C10H14N2 013078-04-1 9 2 Pyridine, 3-(2-piperidinyl)-, (S)- 162 C10H14N2 000494-52-0 9 3 2-Cyclohexen-1-ol, 3-methyl-6-(1... 154 C1OH180 016721-39-4 9 4 2-Propenoic acid, 3-(dimethylami... 212 C11H20N2O2 049582-41-4 8 Abundance Scan 4396 (28.908 min): 11568.D (-4387) (-) m/z 208.90 100.00% 209 84

5000 242 43 61 107 121 135 162 174 . .... A...... 01 1 1 i ■ ■ — I I II, I ‘ * I ‘11." i 1 1 1 1 i ' 1 11 i 1 1 1 1 i1"11 i ' 1 1 1 i 28.60 28.80 29.00 29.20 m/ z 84.00 82.45% n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 • Abundance #33891: DL-Anabasine 84

28 105 5000 119 133 39 51 162 m/z 206.90 67.50%

m/z-> 15 Ot TTI 20 11 4lllqal,LaLlaaiL 40 60 80 100 120 1147 140 160 180 200 220 240 Abundance #116620: Pyridine, 3-(2-piperidinyl)-, (S)- 84 105 1.. 28.60 28.80 29.00 29.20 5000 m/z 241.80 48.17% 119 133 162 39 52 65 I 0+ ■ 1 i 1 --4— —1 147 | — ——— m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #116608:2-Cyclohexen-1-ol, 3-methyl-6-(1-methylethyl)-, t... 84 28.60 28.80 29.00 29.20 m/z 85.90 43.99%

5000

41 121 139 27 । 55

m/z—> 0 mll4 71 I 20 40 60I 80 L 105

100 120 140 154 , I_________________________ i 1 1 11 i 1 l"1 1 1 1 1 ' 1 1 1 11 1 I 1 1 1 1 I । । 160 180 200 220 240 28.60 28.80 29.00 29.20

11568 .D SCAN020521.M Fri May 24 09:42:35 2002 Page 5

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