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GCMS quantitation results for sample AE10241, May 2002

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Laboratory report documenting GCMS analysis of sample AE10241 conducted on May 28, 2002.

NYC-WTC_000024780–000024790

Folder label: “GCMS X 5/14/02 A 5/17/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020509\10241.D Vial: 19 Acq On : 10 May 2002 4:25 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 Phenanthrene, 4-methyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

31.08 0.34 ug/1 42389 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 4-methyl- 192 C15H12 000832-64-4 42 2 Benzene, 1-bromo-2-chloro- 190 C6H4BrCl 000694-80-4 37 3 Benzene, 1-bromo-4-chloro- 190 C6H4BrCl 000106-39-8 37 4 Anthracene, 1-methyl-________________ 192 C15H12 000610-48-0 37 Abundance 7 Scan 4766 (31.082 min): 10241 .D (-4759) (-) m/z 192.05 100.00% 192 M

5000 M 46 57 7084 9 106 122 .1 160 ,I 30,80 31.00 31.20 31.40 TWTTTTTTTTTHtmtthpmpm 1pr m/z 193.00 26.17% m/z—> 10 20 30 40 50 60 70 80 90 100110120130140 150 160 170 180190 200 Abundance #125851: Phenanthrene, 4-methyl- 19/2

5000 30.80 31.00 31.20 31.40 m/z 146.10 17.78% 40 95 165 50 63 82 . 1 125 139 152 J 174 „ TTTTTTTTTTTT r i'l'l I'I'i , "I I p i I I | | | . ...... . i i i rp i i , pl i i i । ) u rr| i i 1 TI’T n/z-> 10 20 30 40 50 60 70 80 90 100110120 130140 150160 170 180190200 Abundance #125837: Benzene, 1-bromo-2-chloro- 192 1 ' । ■ ■ • ■ । ' A 30.80 31.00 31.20 31.40 5000 111 m/Z 94.00 14.39% 75 50 OU OR | 18 28 38 L , 61 I. 85 | 128 141 155 1 I'll IITIgu IT, I'l'l II | I I I I | I I I ! pi I I | I I-I-I | I | I ! | I I I I p | | IT’i | p i I 1 ' " I 1 " 1 1 ' " 1I '" ' !1"1PH' |

m/z—> Abundance 10 20 30 40 50 60 70 80 90 100110120 130140 150160 170 180190 200 #125839: Benzene, 1-bromo-4-chloro- 1912 L 30.80 31.00 31.20 31.40 1 i ‘ 1

m/z 191.10 13.21% 111 5000 75 50 18 28 38 . 61 85 96 A....... II,, 131 155 1 1 । ' ' > ' । ' ■ । । । ' । M /z—> 10 20 30 40 50 60 70 80 90 100110120 130140 150 160 170 180 190 200 30.80 31.00 31.20 31.40

10241.D SCAN020507.M Tue May 14 14:25:38 2002 Page 4

NYC-WTC_000024785

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