GCMS quantitation results for sample AE10241, May 2002

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Data File : C:\MSDCHEM\1\DATA\020509\10241.D Vial: 19 Acq On : 10 May 2002 4:25 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 *********************** * ********************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-me... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 6.15 11.49 ug/1 1025490 1,4-Dichlorobenzene-d4 11.38 . Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4 -hydroxy-4-methyl- 116 C6H1202 000123-42-2 83 2 2- ntanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 50 3 2- ntanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 38 4 2 -Hexanol , 2-methyl- 116 C7H160 000625-23-0 25 Abundance Scan 523 (6.152 min): 10241.D (-518) (-) m/ z 43.05 100.00% 43

5000

101 . , । . i i ; ! i i- i । , [14 r I । i 580 6.00 6.20 6.40 ,,d/a7,,.... ............ .....516 m/z 59.10 51.71% n/z-> 0 50 100 150 200 250 300 350 400 450 500 Abundance #109755:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 ~' ' i ■ 1 ' ........... । 1 । i iT1 ' 1 i । ' 580 6.00 6.20 6.40 m/z 58.05 19.30% 15 101 I .hl ii . ‘I i'tt rp । i1 m/z-> 0 50 100 150 200 250 300 350 400 450 500 Abundance #109756:2-Pentanone, 4-hydroxy-4-methyl- 43 r i 1 ■ ■ 6.00 1 5.80 1 i ■ ■ 1 6.20 ■ । aaandpndi 6.40 । f. 5000 m/z 101.10 16.86%

101 m/z-> 0 50 100 150 200 250 300 350 400 450 500 Abundance #5851:2-Pentanone, 4-hydroxy-4-methyl- **nnn—/—“RTOT 43 580 6.00 6.20 6.40 m/z 41.05 7.66%

5000

101

m/z—> —i 44 —74 TT no M— ImT4e*pr 0 !50 100 150 200 250 300 350 400 450 500 5.80 6.00 6.20 6.40

10241.D SCAN020507.M Tue May 14 14:25:38 2002 Page 3

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