GCMS chain of custody form, sample AE10240, May 2002

Machine-extracted title · confidence 100%

Chain of custody record for GCMS analysis of sample AE10240 on May 20, 2002, including surrogate compound data.

NYC-WTC_000024390–000024401

Folder label: “GCMS X 5/1/02 A 5/9/02”

Page image

OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020509\10240.D Vial: 18 Acq On : 10 May 2002 3:25 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 3,5-Ethanoquinolin-10-ol, d... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

31.09 0.30 ug/1 44332 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3,5-Et anoquinolin-10-ol , decahy. . . 209 C13H23NO 021041-43-0 59 2 4-Hydr xy-3,5-dimethylcinnamic acid 192 C11H1203 1000132-15-8 59 3 Anthra cene, 2-methyl- 192 C15H12 000613-12-7 53 4 Bitoscanate 192 C8H4N2S2 004044-65-9 50 Abundance / Scan 4768 (31.094 min): 10240.D (-4757) (-) m/z 192.10 100.00% 192 h

5000 ...............

44 70 %6 118 146 , 346 30.80 31.00 31.20 31.40 TI—mImuuunuunm—nEnr ■' i" m/z 191.10 20.63% niz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #81097:3,5-Ethanoquinolin-10-ol decahydro-1,7-dimethyl-,... 192

5000 208 11 + J or 44 30.80 31.00 31.20 31.40 166 m/ Z 96.10 14.73%

m/z-> i HH 70 96 — 122 + 150 TT 11' *' I'''11 n '' I'1'11 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ItT

Abundance #81030: 4-Hydroxy-3,5-dimethylcinnamic acid 192 ■ ■ i ■ ■ ■ ■ i h.... ' I ■ ' ' ' I 1 * 30.80 31.00 31.20 31.40 5000 m/z 193.20 14.51% 89 175 45 ? T’TI -4+ e 117 Hii A145 Al 11, ■ ri 111 • j * 11. i.. > ■ । • ■ ■ ■ i ■'' ■ i ■ • ■ * i' ■" i"' • i" ■nfz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #81034: Anthracene, 2-methyl- AA... I ■ ' 1 i 1 ■ ■ 1 i ■ ' * * rr - ...... A 192 30.80 31.00 31.20 31.40 m/ Z 94.10 11.19%

5000

82 165

m/z-> 18.,39 —934198,11513944 ■ i11" i ■"11" " i1"' i11" rr" i1 ■1 ‘ i" 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ■ i ■ ■ ■ । > 30.80 31.00 31.20 31.40

10240.D SCAN020507.M Tue May 14 14:25:25 2002 Page 6

NYC-WTC_000024399

OCR can misread numbers and units. Confirm readings against the page image before using them.

NYC-WTC_000024399Source: NYC Law Department, mirrored locally

Related records

Browse subjects →

Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.

Same-box records

GCMS analysis page for sample AE11571, May 2002 · Box DEP Box 18

NYC-WTC_000025613

GCMS analysis report for sample AE11571 showing unknown compounds and surrogate recovery data from May 29, 2002.

1 shared topics · Same agency, volume and box · similarity 0.997