Laboratory report documenting GCMS analysis of sample AE08324 conducted on May 6, 2002, including surrogate recovery data.
NYC-WTC_000048134–000048147Folder label: “GCMS X 4/9/02 A 4/19/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\1\DATA\020419\08324.D Vial: 11 Acq On : 19 Apr 2002 5:58 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e
Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 5 6,2,5-Ethanylylidene-2H-cyc... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 31.09 0.29 ug/1 631290 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 6,2,5-Ethanylylidene-2H-cyclobut... 192 C11H120S 019086-86-3 40 2 Anthracene, 2-methyl- 000613-12-7 38 192 C15H12 3 Isoquinoline, 1,2,3,4-tetrahydro... 328 C18H20N2O4 1000128-79-2 38 4 Anthracene, 2-methyl- 192 C15H12 000613-12-7 38 Abundance Scan 4768 (31.094 min): 08324. D (-4757) (-) “m/z 192.10 100.00% 192
5000
40 96 146. 30.80 31.00 31.20 31.40 66 82 | 122 | 160 ii M’’i11 ■' ")1 r 1 ■ ■' i '■. 'ii11111 r■ i'' ■ ■ i'' ■11'1'1 ...................................................... 1 ■1 ■ ■ ।11'11''' ■ i' ■ m/z 193.10 22.91% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #80887: 6,2,5-Ethanylylidene-2H-cyclobuta[cd][2]benzothiop... 80 192
5000 59 95 113 30.80 31.00 31.20 31.40 39 m/z 191.10 20.17% 136 163
mz-> 40 60 4.44. 80 100 120 140 160 180 200 220 240 260 280 300 320 i' ■ ■' ir' ■ ■ i ■ ‘1111111111 1 ' 11111 111
Abundance #125845: Anthracene, 2-methyl- 192 1 -p“ ■ i ' ■ 30.80 31.00 31.20 31.40 5000 m/z 96.20 14.40%
96 165 ।
n/z-> 40 mruumpri" A“T 60 75 + 115 199I l-t. l i1 **L I JI 1 11 |/I , . +rri I I > I | I I I I | I' I I 'I | 11 ! I I | 1 I I I | I I I I | I I
80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #81065: Isoquinoline, 1,2,3,4-tetrahydro-1-[2-nitrobenzyl]„. ' ' I 1 1 1 ' I ' 192 30.80 31.00 31.20 31.40 m/z 146.10 13.56%
5000
176 49 63 78 92 117131 148162 1 207 222236250264 280295 311 328 ....... ‘IIT■ 11 ■'1 “i ‘'1' i''1 0'1**i I Tri 1^111" 1 I 1 ' ' ' I ' 7i > I > I | > ' I ' J r I > I | I I I I | 1 > I : ' ' I ' ' ' ' I ' 1 n/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 30.80 31.00 31.20 31.40
08324.D SCAN020418.M Fri May 03 09:04:39 2002 Page 7
NYC-WTC_000048144
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NYC-WTC_000048106
Laboratory report documenting GCMS analysis of sample AE08323 conducted on May 6, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048169
Laboratory report documenting GCMS analysis of sample AE08426 conducted on May 6, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048647
Laboratory report documenting GCMS analysis of sample AE08486 conducted on May 7, 2002, by analyst DLV.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048182
Laboratory report documenting GCMS analysis of sample AE08427 conducted on May 6, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048195
Laboratory report documenting GCMS analysis of sample AE08428 conducted on May 6, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048121
Laboratory report documenting GCMS analysis of sample AE08431 conducted on May 6, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048207
Laboratory report documenting GCMS analysis of sample AE08429 conducted on May 6, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048635
GC/MS analysis report for sample AE08486 conducted May 7, 2002, detecting unknown compounds and surrogate standard 2,4-DDD.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048623
Gas chromatography-mass spectrometry results for sample AE08483 including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048660
Laboratory report documenting GCMS analysis of sample AE08488 conducted on May 7, 2002, by analyst DLV.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047577
Laboratory report documenting GCMS analysis of sample AE07975 conducted on April 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043792
Analytical report for sample AE09768 documenting GC/MS analysis of unknown compounds and surrogate recovery data from May 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000048081
Department of Environmental Protection GCMS analysis record dated April 9-19, 2002.
Filed in the same folder
NYC-WTC_000048082
Fragmented document page containing metadata and identifiers related to GCMS testing procedures from early April 2002.
Filed in the same folder
NYC-WTC_000048085
Laboratory report showing non-detect results for volatile organic compounds in a GCMS blank run (Sample AE08323) from April to May 2002.
Filed in the same folder
NYC-WTC_000048094
Laboratory report of GCMS calibration (Sample AE08323) conducted between April 9 and May 3, 2002, showing response factors for volatile organics.
Filed in the same folder
NYC-WTC_000048098
Laboratory report of GCMS reference standard run (Sample AE08323) conducted between April 9 and May 3, 2002, verifying instrument performance.
Filed in the same folder